Abstract: Cesium molybdates with general formula
CsMIII(MoO4)2, where MIII = Bi, Dy, Pr, Er, exhibit rich
polymorphism, and crystallize in a layered structure. These properties
cause intensive studies on cesium molybdates. CsBi(MoO4)2 was synthesized by microwave method by using
cerium sulphate, bismuth oxide and molybdenum (VI) oxide in an
appropriate molar ratio. Characterizations were done by x-ray
diffraction (XRD), fourier transform infrared (FTIR) spectroscopy,
scanning electron microscopy/energy dispersive analyze (SEM/EDS),
thermo gravimetric/differantial thermal analysis (TG/DTA).
Abstract: An unrecorded experiment of use of the smartphone
as a tool for practical classes of histology is presented in this paper.
Behavior and learning of students of science courses at the University
were analyzed and compared as well as the mode of teaching of this
discipline and the appreciation of the students, using either digital
photographs taken by phone or drawings for record microscopic
observations, analyze and interpret histological sections of human or
animal tissues.
Abstract: The growth in the demand of electrical energy is
leading to load on the Power system which increases the occurrence
of frequent oscillations in the system. The reason for the oscillations
is due to the lack of damping torque which is required to dominate
the disturbances of Power system. By using FACT devices, such as
Unified Power Flow Controller (UPFC) can control power flow,
reduce sub-synchronous resonances and increase transient stability.
Hence, UPFC is used to damp the oscillations occurred in Power
system. This research focuses on adapting the neuro fuzzy controller
for the UPFC design by connecting the infinite bus (SMIB - Single
machine Infinite Bus) to a linearized model of synchronous machine
(Heffron-Phillips) in the power system. This model gains the
capability to improve the transient stability and to damp the
oscillations of the system.
Abstract: A numerical study is made in a parallel-plate porous
channel subjected to an oscillating flow and an exothermic chemical
reaction on its walls. The flow field in the porous region is modeled
by the Darcy–Brinkman–Forchheimer model and the finite volume
method is used to solve the governing equations. The effects of the
modified Frank-Kamenetskii (FKm) and Damköhler (Dm) numbers,
the amplitude of oscillation (A), and the Strouhal number (St) are
examined. The main results show an increase of heat and mass
transfer rates with A and St, and their decrease with FKm and Dm.
Abstract: The present study deals with the characterization of
CrSiN coatings obtained by PVD magnetron sputtering systems.
CrSiN films were deposited with different Si contents, in order to
check the effect of at.% variation on the different properties of the
Cr–N system. Coatings were characterized by scanning electron
microscopy (SEM) for thickness measurements, X-ray diffraction.
Surface morphology and the roughness characteristics were explored
using AFM, Mechanicals properties, elastic and plastic deformation
resistance of thin films were investigated using nanoindentation test. We observed that the Si addition improved the hardness and the
Young’s modulus of the Cr–N system. Indeed, the hardness value is
18,56 GPa for CrSiN coatings. Besides, the Young’s modulus value
is 224,22 GPa for CrSiN coatings for Si content of 1.2 at.%.
Abstract: The ferrites ZnFe2O4, CdFe2O4 and CuFe2O4 are
synthesized in laboratory conditions using ceramic technology. Their
homogeneity and structure are proven by X-Ray diffraction analysis
and Mössbauer spectroscopy. The synthesized ferrites are subjected
to strong acid and high temperature leaching with solutions of H2SO4,
HCl and HNO3. The results indicate that the highest degree of
leaching of Zn, Cd and Cu from the ferrites is achieved by use of
HCl. The charging of five zinc sulfide concentrates was optimized using
the criterion of minimal amount of zinc ferrite produced when
roasting the concentrates in a fluidized bed. The results obtained are
interpreted in terms of the hydrometallurgical zinc production and
maximum recovery of zinc, copper and cadmium from initial zinc
concentrates after their roasting.
Abstract: Friction stir welding and tungsten inert gas welding
techniques were employed to weld armor grade aluminum alloy to
investigate the effect of welding processes on tensile behavior of
weld joints. Tensile tests, Vicker microhardness tests and optical
microscopy were performed on developed weld joints and base metal.
Welding process influenced tensile behavior and microstructure of
weld joints. Friction stir welded joints showed tensile behavior better
than tungsten inert gas weld joints.
Abstract: One of the tasks of optical surveillance is to detect
anomalies in large amounts of image data. However, if the size of the
anomaly is very small, limited information is available to distinguish
it from the surrounding environment. Spectral detection provides a
useful source of additional information and may help to detect
anomalies with a size of a few pixels or less. Unfortunately, spectral
cameras are expensive because of the difficulty of separating two
spatial in addition to one spectral dimension. We investigate the
possibility of modifying a simple spectral line detector for outdoor
detection. This may be especially useful if the area of interest forms a
line, such as the horizon. We use a monochrome CCD that also
enables detection into the near infrared. A simple camera is attached
to the setup to determine which part of the environment is spectrally
imaged. Our preliminary results indicate that sensitive detection of
very small targets is indeed possible. Spectra could be taken from the
various targets by averaging columns in the line image. By imaging a
set of lines of various widths we found narrow lines that could not be
seen in the color image but remained visible in the spectral line
image. A simultaneous analysis of the entire spectra can produce
better results than visual inspection of the line spectral image. We are
presently developing calibration targets for spatial and spectral
focusing and alignment with the spatial camera. This will present
improved results and more use in outdoor application.
Abstract: Zinc borate is an important inorganic hydrate borate
material, which can be used as a flame retardant agent and corrosion
resistance material. This compound can loss its structural water
content at higher than 290°C. Due to thermal stability; Zinc Borate
can be used as flame retardant at high temperature process of plastic
and gum. In this study, the ultrasonic reaction of zinc borates were
studied using hydrozincite (Zn5(CO3)2·(OH)6) and boric acid
(H3BO3) raw materials. Before the synthesis raw materials were
characterized by X-Ray Diffraction (XRD) and Fourier Transform
Infrared Spectroscopy (FT-IR). Ultrasonic method is a new
application on the zinc borate synthesis. The synthesis parameters
were set to 90°C reaction temperature and 55 minutes of reaction
time, with 1:1, 1:2, 1:3, 1:4 and 1:5 molar ratio of starting materials
(Zn5(CO3)2·(OH)6 : H3BO3). After the zinc borate synthesis, the
products were analyzed by XRD and FT-IR. As a result, optimum
molar ratio of 1:5 is determined for the synthesis of zinc borates with
ultrasonic method.
Abstract: This paper presents the result of an experimental
investigation regarding the use of Fe2O3 nanoparticles added to
kerosene as a working fluid, under magnetic field for Copper
Oscillating Heat pipe with inclination angle of 0°(horizontal), 15°,
30°,45°, 60°,75° and 90° (vertical). The following were examined;
measure the temperature distribution and heat transfer rate on
Oscillating Heat Pipe (OHP), with magnetic field under different
angles. Results showed that the addition of Fe2O3 nanoparticles under
magnetic field improved thermal performance of OHP especially in
75°.
Abstract: This paper proposes for the first time symbolic
formula of the power spectrum of CMOS Cross Couple Oscillator
and its modified circuit. Many principles existed to derived power
spectrum in microwave textbook such as impedance, admittance
parameters, ABCD, H parameters, etc. It can be compared by graph
of power spectrum which methodology is the best from the point of
view of practical measurement setup such as condition of impedance
parameter which used superposition of current to derived (its current
injection at the other port of the circuit is zero, which is impossible in
reality). Four graphs of impedance parameters of cross couple
oscillator are proposed. After that four graphs of scattering
parameters of CMOS cross coupled oscillator will be shown.
Abstract: Ceramic obtained on the base of aluminum oxide has
wide application range, because it has unique properties, for example,
wear-resistance, dielectric characteristics, and exploitation ability at
high temperatures and in corrosive atmosphere. Low temperature
synthesis of α-Al2O3 is energo-economical process and it is topical
for developing technologies of corundum ceramics fabrication. In the present work possibilities of low temperature transformation
of oxyhydroxides in α-Al2O3, during the presence of small amount of
rare–earth elements compounds (also Th, Re), have been discussed.
Aluminum unstable oxyhydroxides have been obtained by hydrolysis
of aluminium isopropoxide, nitrates, sulphate, and chloride in
alkaline environment at 80-90ºC temperatures. β-Al(OH)3 has been
received from aluminum powder by ultrasonic development. Drying
of oxyhydroxide sol has been conducted with presence of various
types seeds, which amount reaches 0,1-0,2% (mas). Neodymium,
holmium, thorium, lanthanum, cerium, gadolinium, disprosium
nitrates and rhenium carbonyls have been used as seeds and they
have been added to the sol specimens in amount of 0.1-0.2% (mas)
calculated on metals. Annealing of obtained gels is carried out at 70–
1100ºC for 2 hrs. The same specimen transforms in α-Al2O3 at
1100ºC. At this temperature in case of presence of lanthanum and
gadolinium transformation takes place by 70-85%. In case of
presence of thorium stabilization of γ-and θ-phases takes place. It is
established, that thorium causes inhibition of α-phase generation at
1100ºC, and at the time when in all other doped specimens α-phase is
generated at lower temperatures (1000-1050ºC). Synthesis of various
type compounds and simultaneous consolidation has developed in the
furnace of OXY-GON. Composite materials containing oxide and
non-oxide components close to theoretical data have been obtained in
this furnace respectively. During the work the following devices have
been used: X-ray diffractometer DRON-3M (Cu-Kα, Ni filter,
2º/min), High temperature vacuum furnace OXY-GON, electronic
scanning microscopes Nikon ECLIPSE LV 150, NMM-800TRF,
planetary mill Pulverisette 7 premium line, SHIMADZU Dynamic
Ultra Micro Hardness Tester, DUH-211S, Analysette 12 Dyna sizer.
Abstract: Nonlinear evolution of broadband ultrasonic pulses
passed through the rock specimens is studied using the apparatus
“GEOSCAN-02M”. Ultrasonic pulses are excited by the pulses of Qswitched
Nd:YAG laser with the time duration of 10 ns and with the
energy of 260 mJ. This energy can be reduced to 20 mJ by some light
filters. The laser beam radius did not exceed 5 mm. As a result of the
absorption of the laser pulse in the special material – the optoacoustic
generator–the pulses of longitudinal ultrasonic waves are excited with
the time duration of 100 ns and with the maximum pressure
amplitude of 10 MPa. The immersion technique is used to measure
the parameters of these ultrasonic pulses passed through a specimen,
the immersion liquid is distilled water. The reference pulse passed
through the cell with water has the compression and the rarefaction
phases. The amplitude of the rarefaction phase is five times lower
than that of the compression phase. The spectral range of the
reference pulse reaches 10 MHz. The cubic-shaped specimens of the
Karelian gabbro are studied with the rib length 3 cm. The ultimate
strength of the specimens by the uniaxial compression is (300±10)
MPa. As the reference pulse passes through the area of the specimen
without cracks the compression phase decreases and the rarefaction
one increases due to diffraction and scattering of ultrasound, so the
ratio of these phases becomes 2.3:1. After preloading some horizontal
cracks appear in the specimens. Their location is found by one-sided
scanning of the specimen using the backward mode detection of the
ultrasonic pulses reflected from the structure defects. Using the
computer processing of these signals the images are obtained of the
cross-sections of the specimens with cracks. By the increase of the
reference pulse amplitude from 0.1 MPa to 5 MPa the nonlinear
transformation of the ultrasonic pulse passed through the specimen
with horizontal cracks results in the decrease by 2.5 times of the
amplitude of the rarefaction phase and in the increase of its duration
by 2.1 times. By the increase of the reference pulse amplitude from 5
MPa to 10 MPa the time splitting of the phases is observed for the
bipolar pulse passed through the specimen. The compression and
rarefaction phases propagate with different velocities. These features
of the powerful broadband ultrasonic pulses passed through the rock
specimens can be described by the hysteresis model of Preisach-
Mayergoyz and can be used for the location of cracks in the optically
opaque materials.
Abstract: Si-Ge solid solutions (bulk poly- and mono-crystalline
samples, thin films) are characterized by high perspectives for
application in semiconductor devices, in particular, optoelectronics
and microelectronics. From this point of view, complex studying of
structural state of the defects and structural-sensitive physical
properties of Si-Ge solid solutions depending on the contents of Si
and Ge components is very important. Present work deals with the
investigations of microstructure, microhardness, internal friction and
shear modulus of Si1-xGex(x≤0,02) bulk monocrystals conducted at
room temperature. Si-Ge bulk crystals were obtained by Czochralski
method in [111] crystallographic direction. Investigated
monocrystalline Si-Ge samples are characterized by p-type
conductivity and carriers’ concentration 5.1014-1.1015cm-3.
Microhardness was studied on Dynamic Ultra Micro hardness Tester
DUH-201S with Berkovich indenter. Investigate samples are characterized with 0,5x0,5x(10-15)mm3
sizes, oriented along [111] direction at torsion oscillations ≈1Hz,
multistage changing of internal friction and shear modulus has been
revealed in an interval of strain amplitude of 10-5-5.10-3. Critical
values of strain amplitude have been determined at which hysteretic
changes of inelastic characteristics and microplasticity are observed. The critical strain amplitude and elasticity limit values are also
determined. Dynamic mechanical characteristics decreasing trend is
shown with increasing Ge content in Si-Ge solid solutions. Observed
changes are discussed from the point of view of interaction of various
dislocations with point defects and their complexes in a real structure
of Si-Ge solid solutions.
Abstract: Ocean current is always available around the
surrounding of SHELL Sabah Water Platform and data are collected
every 10 minutes, 24 hours a day, for a period of 365 days. Due to
low current speed, conventional hydrokinetic power generation is not
feasible, thus leading to the study of low current enabled vortex
induced vibration power generation application. In this case, the
design of a vortex induced vibration application is studied to obtain
an optimum design for the VIV oscillator. Power output is then
determined to study the feasibility of the VIV application in low
current condition.
Abstract: The growing concerns for physical wellbeing and
health have been reflected in the way we choose food in our table.
Nowadays, we are all more informed consumers and choose healthier
foods. On the other hand, stroke, cancer and atherosclerosis may be
somehow minimized by the intake of some bioactive compounds
present in food, the so-called nutraceuticals and functional foods. The
aim of this work was to make a revision of the published studies
about the effects of some bioactive compounds, namely lycopene in
human health, in the prevention of diseases, thus playing the role of a
functional food. Free radical in human body can induce cell damage
and consequently can be responsible for the development of some
cancers and chronic diseases. Lycopene is one of the most powerful
antioxidants known, being the predominant carotenoid in tomato. The
respective chemistry, bioavailability, and its functional role in the
prevention of several diseases will be object of this work. On the
other hand, the inclusion of lycopene in some foods can also be made
by biotechnology and represents a way to recover the wastes in the
tomato industry with nutritional positive effects in health.
Abstract: Carbon nanotubes (CNTs) are known for having high elastic properties with high surface area that promote them as good candidates for reinforcing polymeric matrices. In composite materials, CNTs lack chemical bonding with the surrounding matrix which decreases the possibility of better stress transfer between the components. In this work, a chemical treatment for activating the surface of the multi-wall carbon nanotubes (MWCNT) was applied and the effect of this functionalization on the elastic properties of the epoxy nanocomposites was studied. Functional amino-groups were added to the surface of the CNTs and it was evaluated to be about 34% of the total weight of the CNTs. Elastic modulus was found to increase by about 40% of the neat epoxy resin at CNTs’ weight fraction of 0.5%. The elastic modulus was found to decrease after reaching a certain concentration of CNTs which was found to be 1% wt. The scanning electron microscopic pictures showed the effect of the CNTs on the crack propagation through the sample by forming stress concentrated spots at the nanocomposite samples.
Abstract: This paper reports the viability of developing Zn-27Al
alloy matrix hybrid composites reinforced with alumina, graphite and
fly ash (solid waste bye product of coal in thermal power plants).
This research work was aimed at developing low cost-high
performance Zn-27Al matrix composite with low density. Alumina
particulates (Al2O3), graphite added with 0, 2, 3, 4 and 5 wt% fly ash
were utilized to prepare 10wt% reinforcing phase with Zn-27Al alloy
as matrix using two-step stir casting method. Density measurement,
estimated percentage porosity, tensile testing, micro hardness
measurement and optical microscopy were used to assess the
performance of the composites produced. The results show that the
hardness, ultimate tensile strength, and percent elongation of the
hybrid composites decrease with increase in fly ash content. The
maximum decrease in hardness and ultimate tensile strength of
13.72% and 15.25% respectively were observed for composite grade
containing 5wt% fly ash. The percentage elongation of composite
sample without fly ash is 8.9% which is comparable with that of the
sample containing 2wt% fly ash with percentage elongation of 8.8%.
The fracture toughness of the fly ash containing composites was
however superior to those of composites without fly ash with 5wt%
fly ash containing composite exhibiting the highest fracture
toughness. The results show that fly ash can be utilized as
complementary reinforcement in ZA-27 alloy matrix composite to
reduce cost.
Abstract: The consumption of food contaminated with molds
(microscopic filamentous fungi) and their toxic metabolites results in
the development of food-borne mycotoxicosis. The spores of molds
are ubiquitously spread in the environment and can be detected
everywhere. Ochratoxin A is a toxic and potentially carcinogenic
fungal toxin found in a variety of food commodities. In this study, the
mycological quality of various ready-to-eat local and imported pork
meat and meat byproducts sold in Egyptian markets were assessed
and the presence of various molds was determined in pork used as a
raw material, edible organs as liver and kidney as well as in
fermented raw meat by-products. The study assessed the mycological
quality of pork raw meat and their by-products sold in commercial
shops in Cairo, Egypt. Mycological analysis was conducted on
(n=110) samples which included pig’s livers and kidneys from
Egyptian Bassatin slaughter house; local and imported processed
pork meat by-products from Egyptian pork markets. The isolates
were identified using traditional mycological and biochemical tests.
All kidney and liver samples were positive to molds growth while all
byproducts were negative. Ochratoxin A levels were quantitatively
analyzed using the high performance liquid chromatography (HPLC)
and the highest results were present in kidney 7.51 part per billion
(ppb) followed by minced meat 6.19 ppb generally the local samples
showed higher levels than the imported ones. To the best of our
knowledge, this is the first report on mycotoxins detection and
quantification from pork by-products in Egypt.
Abstract: This paper reports on the response of a fiber-optic
sensing probe to small concentrations of hydrogen peroxide (H2O2)
vapor at room temperature. H2O2 has extensive applications in industrial and medical
environments. Conversely, H2O2 can be a health hazard by itself. For
example, H2O2 induces cellular damage in human cells and its
presence can be used to diagnose illnesses such as asthma and human
breast cancer. Hence, development of reliable H2O2 sensor is of vital
importance to detect and measure this species. Ferric ferrocyanide, referred to as Prussian Blue (PB), was
deposited on the tip of a multimode optical fiber through the single
source precursor technique and served as an indicator of H2O2 in a
spectroscopic manner. Sensing tests were performed in H2O2-H2O
vapor mixtures with different concentrations of H2O2. The results of sensing tests show the sensor is able to detect H2O2
concentrations in the range of 50.6 ppm to 229.5 ppm. Furthermore,
the sensor response to H2O2 concentrations is linear in a log-log scale
with the adjacent R-square of 0.93. This sensing behavior allows us
to detect and quantify the concentration of H2O2 in the vapor phase.