Abstract: Zinc borates can be used as multi-functional
synergistic additives with flame retardant additives in polymers. Zinc
borate is white, non-hygroscopic and powder type product. The most
important properties are low solubility in water and high dehydration
temperature. Zinc borates dehydrate above 290°C and anhydrous zinc
borate has thermal resistance about 400°C. Zinc borates can be
synthesized using several methods such as hydrothermal and solidstate
processes. In this study, the solid-state method was applied at
low temperatures of 600oC and 700oC using the starting materials of
ZnO and H3BO3 with several mole ratios. The reaction time was
determined as 4 hours after some preliminary experiments. After the
synthesis, the crystal structure and the morphology of the products
were examined by X-Ray Diffraction (XRD) and Fourier Transform
Infrared Spectroscopy (FT-IR). As a result the forms of ZnB4O7,
Zn3(BO3)2, ZnB2O4 were synthesized and obtained along with the
unreacted ZnO.
Abstract: Utilization of bagasse ash for silica sources is one of
the most common application for agricultural wastes and valuable
biomass byproducts in sugar milling. The high percentage silica
content from bagasse ash was used as silica source for sodium
silicate solution. Different heating temperature, time and acid
treatment were studies for silica extraction. The silica was
characterized using various techniques including X-ray fluorescence,
X-ray diffraction, Scanning electron microscopy, and Fourier
Transform Infrared Spectroscopy method,. The synthesis conditions
were optimized to obtain the bagasse ash with the maximum silica
content. The silica content of 91.57 percent was achieved from
heating of bagasse ash at 600°C for 3 hours under oxygen feeding
and HCl treatment. The result can be used as value added for bagasse
ash utilization and minimize the environmental impact of disposal
problems.
Abstract: The article examines the methods of protection of
citizens' personal data on the Internet using biometric identity
authentication technology. It`s celebrated their potential danger due
to the threat of loss of base biometric templates. To eliminate the
threat of compromised biometric templates is proposed to use neural
networks large and extra-large sizes, which will on the one hand
securely (Highly reliable) to authenticate a person by his biometrics,
and on the other hand make biometrics a person is not available for
observation and understanding. This article also describes in detail
the transformation of personal biometric data access code. It`s formed
the requirements for biometrics converter code for his work with the
images of "Insider," "Stranger", all the "Strangers". It`s analyzed the
effect of the dimension of neural networks on the quality of
converters mystery of biometrics in access code.
Abstract: In this paper an efficient incomplete factorization preconditioner is proposed for the Least Mean Squares (LMS) adaptive filter. The proposed preconditioner is approximated from a priori knowledge of the factors of input correlation matrix with an incomplete strategy, motivated by the sparsity patter of the upper triangular factor in the QRD-RLS algorithm. The convergence properties of IPLMS algorithm are comparable with those of transform domain LMS(TDLMS) algorithm. Simulation results show efficiency and robustness of the proposed algorithm with reduced computational complexity.
Abstract: This research was conducted to develop a correlation
between microstructure of HSLA steel and the mechanical properties
that occur as a result of both laser and mechanical forming processes
of the metal. The technique of forming flat metals by applying laser
beams is a relatively new concept in the manufacturing industry.
However, the effects of laser energy on the stability of metal alloy
phases have not yet been elucidated in terms of phase
transformations and microhardness. In this work, CO2 laser source
was used to irradiate the surface of a flat metal then the
microstructure and microhardness of the metal were studied on the
formed specimen. The extent to which the microstructure changed
depended on the heat inputs of up to 1000 J/cm2 with cooling rates of
about 4.8E+02 K/s. Experimental results revealed that the irradiated
surface of a HSLA steel had transformed to austenitic structure
during the heating process.
Abstract: In this paper the direct kinematic model of a multiple
applications three degrees of freedom industrial manipulator, was
developed using the homogeneous transformation matrices and the
Denavit - Hartenberg parameters, likewise the inverse kinematic
model was developed using the same method, verifying that in the
workload border the inverse kinematic presents considerable errors,
therefore a genetic algorithm was implemented to optimize the model
improving greatly the efficiency of the model.
Abstract: This paper presents a signal analysis process for
improving energy completeness based on the Hilbert-Huang
Transform (HHT). Firstly, the vibration signal of a DC Motor obtained
by employing an accelerometer is the model used to analyze the
signal. Secondly, the intrinsic mode functions (IMFs) and Hilbert
spectrum of the decomposed signal are obtained by applying HHT.
The results of the IMFs constituent and the original signal are
compared and the process of energy loss is discussed. Finally, the
differences between Wavelet Transform (WT) and HHT in analyzing
the signal are compared. The simulated results reveal the analysis
process based on HHT is advantageous for the enhancement of energy
completeness.
Abstract: In this paper, a novel feature-based image
watermarking scheme is proposed. Zernike moments which have
invariance properties are adopted in the scheme. In the proposed
scheme, feature points are first extracted from host image and several
circular patches centered on these points are generated. The patches
are used as carriers of watermark information because they can be
regenerated to locate watermark embedding positions even when
watermarked images are severely distorted. Zernike transform is then
applied to the patches to calculate local Zernike moments. Dither
modulation is adopted to quantize the magnitudes of the Zernike
moments followed by false alarm analysis. Experimental results show
that quality degradation of watermarked image is visually
transparent. The proposed scheme is very robust against image
processing operations and geometric attacks.
Abstract: The paper deals with cartographic visualisation of
results of transport accessibility monitoring with the use of a semiautomated
method of unipolar anamorphosis, developed by the
authors in the GIS environment. The method is based on
transformation of distance in the map to values of a geographical
phenomenon. In the case of time accessibility it is based on
transformation of isochrones converted into the form of concentric
circles, taking into account selected topographic and thematic
elements in the map. The method is most suitable for analyses of
accessibility to or from a centre and for modelling its long-term
context.
The paper provides a detailed analysis of the procedures and
functionality of the method, discussing the issues of coordinates,
transformation, scale and visualisation. It also offers a discussion of
possible problems and inaccuracies. A practical application of the
method is illustrated by previous research results by the authors in
the filed of accessibility in Czechia.
Abstract: The behavior of three phase five leg transformer under voltage sag is studied in this paper. This paper proposes a simple, practical model of a three phase-five leg, saturated transformer with accurate performance. Transformer saturation is produced when the voltage sag is recovered and it causes inrush current in transformer. Effects of voltage sag depth, duration and initial point on wave have been analyzed in this paper. Initial point on wave can produce maximum inrush current in five leg transformers while comparing with three leg transformers. The magnetic circuit symmetry of five leg transformer produces the more symmetrical shape of inrush current curves versus initial point on wave and sag duration than three leg transformer. The simulations show that current peak has a periodical dependence on sag duration and linear dependence on sag depth. Inrush current that is produced in three phase five leg transformer is higher than three phase three leg transformer.
Abstract: The complex structure of lignocellulose leads to great
difficulties in converting it to fermentable sugars for the ethanol
production. The major hydrolysis impediments are the crystallinity of
cellulose and the lignin content. To improve the efficiency of
enzymatic hydrolysis, microbial pretreatment of corncob was
investigated using two bacterial strains of Bacillus subtilis A 002 and
Cellulomonas sp. TISTR 784 (expected to break open the crystalline
part of cellulose) and lignin-degrading fungus, Phanerochaete
sordida SK7 (expected to remove lignin from lignocellulose). The
microbial pretreatment was carried out with each strain under its
optimum conditions. The pretreated corncob samples were further
hydrolyzed to produce reducing glucose with low amounts of
commercial cellulase (25 U·g-1 corncob) from Aspergillus niger. The
corncob samples were determined for composition change by X-ray
diffraction (XRD), Fourier transform infrared spectroscopy (FTIR),
and scanning electron microscope (SEM). According to the results,
the microbial pretreatment with fungus, P. sordida SK7 was the most
effective for enhancing enzymatic hydrolysis, approximately, 40%
improvement.
Abstract: The hybrid membranes containing inorganic materials in polymer matrix are identified as a remarkable family of proton conducting hybrid electrolytes. In this work, the proton conducting inorganic/organic hybrid membranes for proton exchange membrane fuel cells (PEMFCs) were prepared using polyvinyl alcohol (PVA), tetraethoxyorthosilane (TEOS) and heteropolyacid (HPA). The synthesized hybrid membranes were characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction spectroscopy (XRD), Scanning electron microscopy (SEM) and Thermogravimetry analysis (TGA). The effects of heteropolyacid incorporation on membrane properties, including morphology and thermal stability were extensively investigated.
Abstract: The development of aid's systems for the medical
diagnosis is not easy thing because of presence of inhomogeneities in
the MRI, the variability of the data from a sequence to the other as
well as of other different source distortions that accentuate this
difficulty. A new automatic, contextual, adaptive and robust
segmentation procedure by MRI brain tissue classification is
described in this article. A first phase consists in estimating the
density of probability of the data by the Parzen-Rozenblatt method.
The classification procedure is completely automatic and doesn't
make any assumptions nor on the clusters number nor on the
prototypes of these clusters since these last are detected in an
automatic manner by an operator of mathematical morphology called
skeleton by influence zones detection (SKIZ). The problem of
initialization of the prototypes as well as their number is transformed
in an optimization problem; in more the procedure is adaptive since it
takes in consideration the contextual information presents in every
voxel by an adaptive and robust non parametric model by the
Markov fields (MF). The number of bad classifications is reduced by
the use of the criteria of MPM minimization (Maximum Posterior
Marginal).
Abstract: Power Spectral Density (PSD) computed by taking the Fourier transform of auto-correlation functions (Wiener-Khintchine Theorem) gives better result, in case of noisy data, as compared to the Periodogram approach. However, the computational complexity of Wiener-Khintchine approach is more than that of the Periodogram approach. For the computation of short time Fourier transform (STFT), this problem becomes even more prominent where computation of PSD is required after every shift in the window under analysis. In this paper, recursive version of the Wiener-Khintchine theorem has been derived by using the sliding DFT approach meant for computation of STFT. The computational complexity of the proposed recursive Wiener-Khintchine algorithm, for a window size of N, is O(N).
Abstract: Low silica type X (LSX) Zeolite is one of useful
material in many manufacturing due to the advantage properties
including high surface area, stability, microporous crystalline
aluminosilicates and positive ion in an extra–framework. The LSX
was used rice husk silica source which obtained by leaching with
hydrochloric acid and calcination at 500 C. To improve the
synthesis method, the LSX was crystallizated in Teflon–lined
autoclave will expedite deceasing of the amorphous particles. The
mixed gel with composition of 5.5 Na2O : 1.65 K2O : Al2O3 : 2.2
SiO2 : 122 H2O was crystallized in different container
(Polypropylene bottom and Teflon–lined autoclave). The obtained
powder was characterized by X–ray diffraction (XRD), X–ray
fluorescence spectrometry, N2 adsorption-desorption analysis BET
surface area Scanning electron microscopy (SEM) and Fourier
transform infrared spectroscopy to justify the quality of zeolite. The
results showed the crystallized zeolite in Teflon lined autoclave has
102.8 nm of crystal size, 286 m2/g of surface area and fewer amounts
of round amorphous particles when compared with the crystallized
zeolite in Polypropylene.
Abstract: In this article an isotropic linear elastic half-space with
a cylindrical cavity of finite length is considered to be under the
effect of a ring shape time-harmonic torsion force applied at an
arbitrary depth on the surface of the cavity. The equation of
equilibrium has been written in a cylindrical coordinate system. By
means of Fourier cosine integral transform, the non-zero
displacement component is obtained in the transformed domain. With
the aid of the inversion theorem of the Fourier cosine integral
transform, the displacement is obtained in the real domain. With the
aid of boundary conditions, the involved boundary value problem for
the fundamental solution is reduced to a generalized Cauchy singular
integral equation. Integral representation of the stress and
displacement are obtained, and it is shown that their degenerated
form to the static problem coincides with existing solutions in the
literature.
Abstract: In this paper, a semi-fragile watermarking scheme is proposed for color image authentication. In this particular scheme, the color image is first transformed from RGB to YST color space, suitable for watermarking the color media. Each channel is divided into 4×4 non-overlapping blocks and its each 2×2 sub-block is selected. The embedding space is created by setting the two LSBs of selected sub-block to zero, which will hold the authentication and recovery information. For verification of work authentication and parity bits denoted by 'a' & 'p' are computed for each 2×2 subblock. For recovery, intensity mean of each 2×2 sub-block is computed and encoded upto six to eight bits depending upon the channel selection. The size of sub-block is important for correct localization and fast computation. For watermark distribution 2DTorus Automorphism is implemented using a private key to have a secure mapping of blocks. The perceptibility of watermarked image is quite reasonable both subjectively and objectively. Our scheme is oblivious, correctly localizes the tampering and able to recovery the original work with probability of near one.
Abstract: This paper looks into areas not covered by prominent
Agent-Oriented Software Engineering (AOSE) methodologies.
Extensive paper review led to the identification of two issues, first
most of these methodologies almost neglect semantic web and
ontology. Second, as expected, each one has its strength and
weakness and may focus on some phases of the development
lifecycle but not all of the phases. The work presented here builds
extensions to a highly regarded AOSE methodology (MaSE) in order
to cover the areas that this methodology does not concentrate on. The
extensions include introducing an ontology stage for semantic
representation and integrating early requirement specification from a
methodology which mainly focuses on that. The integration involved
developing transformation rules (with the necessary handling of nonmatching
notions) between the two sets of representations and
building the software which automates the transformation. The
application of this integration on a case study is also presented in the
paper. The main flow of MaSE stages was changed to smoothly
accommodate the new additions.
Abstract: In this paper processes including large deformations of a rubber with hyperelastic material behavior are simulated by the RKPM method. Due to the loss of kronecker delta properties in the mesh less shape functions, the imposition of essential boundary conditions consumes significant CPU time in mesh free computations. In this work transformation method is used for imposition of essential boundary conditions. A RKPM material shape function is used in this analysis. The support of the material shape functions covers the same set of particles during material deformation and hence the transformation matrix is formed only once at the initial stages. A computer program in MATLAB is developed for simulations.
Abstract: In this study, multiwall carbon nanotubes (MWNTs)
were modified with nitric acid chemically and by dielectric barrier
discharge (DBD) plasma in an oxygen-based atmosphere. Used
carbon nanotubes (CNTs) were prepared by chemical vapour
deposition (CVD) floating catalyst method. For removing amorphous
carbon and metal catalyst, MWNTs were exposed to dry air and
washed with hydrochloric acid. Heating purified CNTs under helium
atmosphere caused elimination of acidic functional groups. Fourier
transformed infrared spectroscopy (FTIR) shows formation of
oxygen containing groups such as C=O and COOH. Brunauer,
Emmett, Teller (BET) analysis revealed that functionalization causes
generation of defects on the sidewalls and opening of the ends of
CNTs. Results of temperature-programmed desorption (TPD) and gas
chromatography(GC) indicate that nitric acid treatment create more
acidic groups than plasma treatment.