Abstract: High Performance Liquid Chromatography (HPLC)
method was developed and validated for simultaneous estimation of
6-Gingerol(6G) and 6-Shogaol(6S) in joint pain relief gel containing
ginger extract. The chromatographic separation was achieved by
using C18 column, 150 x 4.6mm i.d., 5μ Luna, mobile phase
containing acetonitrile and water (gradient elution). The flow rate
was 1.0 ml/min and the absorbance was monitored at 282 nm. The
proposed method was validated in terms of the analytical parameters
such as specificity, accuracy, precision, linearity, range, limit of
detection (LOD), limit of quantification (LOQ), and determined
based on the International Conference on Harmonization (ICH)
guidelines. The linearity ranges of 6G and 6S were obtained over 20-
60 and 6-18 μg/ml respectively. Good linearity was observed over the
above-mentioned range with linear regression equation Y= 11016x-
23778 for 6G and Y = 19276x-19604 for 6S (x is concentration of
analytes in μg/ml and Y is peak area). The value of correlation
coefficient was found to be 0.9994 for both markers. The limit of
detection (LOD) and limit of quantification (LOQ) for 6G were
0.8567 and 2.8555 μg/ml and for 6S were 0.3672 and 1.2238 μg/ml
respectively. The recovery range for 6G and 6S were found to be
91.57 to 102.36 % and 84.73 to 92.85 % for all three spiked levels.
The RSD values from repeated extractions for 6G and 6S were 3.43
and 3.09% respectively. The validation of developed method on
precision, accuracy, specificity, linearity, and range were also
performed with well-accepted results.
Abstract: The increase of technogenic and natural accidents,
accompanied by air pollution, for example, by combustion products,
leads to the necessity of respiratory protection. This work is devoted to the development of a calorimetric method
and a device which allows investigating quickly the kinetics of
carbon dioxide sorption by chemisorbents on the base of potassium
superoxide in order to assess the protective properties of respiratory
protective closed circuit apparatus. The features of the traditional approach for determining the
sorption properties in a thin layer of chemisorbent are described, as
well as methods and devices, which can be used for the sorption
kinetics study. The authors developed an approach (as opposed to the traditional
approach) based on the power measurement of internal heat sources
in the chemisorbent layer. The emergence of the heat sources is a
result of exothermic reaction of carbon dioxide sorption. This
approach eliminates the necessity of chemical analysis of samples
and can significantly reduce the time and material expenses during
chemisorbents testing. Error of determining the volume fraction of adsorbed carbon
dioxide by the developed method does not exceed 12%. Taking into
account the efficiency of the method, we consider that it is a good
alternative to traditional methods of chemical analysis under the
assessment of the protection sorbents quality.
Abstract: Effective internal control system in the bursary unit of
tertiary educational institutions is geared toward achieving quality
teaching, learning and research environment and as well assist the
management of the institutions, particularly when decisions are to be
made. While internal control system exists in all institutions, the
outlined objectives above are far from being achieved. The paper
therefore assesses the effectiveness of internal control system in
tertiary educational institutions in Nasarawa State, Nigeria with
specific focus on the Nasarawa State Polytechnic, Lafia. The study is
survey, hence a simple closed ended questionnaire was developed
and administered to a sample of twenty seven (27) member staff from
the Bursary and the Internal audit unit of the Nasarawa State
Polytechnic, Lafia so as to obtain data for analysis purposes and to
test the study hypothesis. Responses from the questionnaire were
analysed using a simple percentage and chi square. Findings shows
that the right people are not assigned to the right job in the
department, budget, and management accounting were never used in
the institution’s operations and checking of subordinate by their
superior officers is not regular. This renders the current internal
control structure of the Polytechnic as ineffective and weak. The
paper therefore recommends that: transparency should be seen as
significant, as the institution work toward meeting its objectives, it
therefore means that the right staff be assigned the right job and
regular checking of the subordinates by their superiors be ensued.
Abstract: Internal circulation two-platen clamping system for
injection molding machine (IMM) has many potential advantages on
energy-saving. In order to estimate its properties, experiments were
carried out in this paper. Displacement and pressure of the components
were measured. In comparison, the model of hydraulic clamping
system was established by using AMESim. The related parameters as
well as the energy consumption could be calculated. According to the
analysis, the hydraulic system was optimized in order to reduce the
energy consumption.
Abstract: Radio Frequency Identification (RFID) has become a
key technology in the emerging concept of Internet of Things (IoT).
Naturally, business applications would require the deployment of
various RFID systems developed by different vendors that use
different data formats and structures. This heterogeneity poses a
challenge in developing real-life IoT systems with RFID, as
integration is becoming very complex and challenging. Semantic
integration is a key approach to deal with this challenge. To do so,
ontology for RFID systems need to be developed in order to
annotated semantically RFID systems, and hence, facilitate their
integration. Accordingly, in this paper, we propose ontology for
RFID systems. The proposed ontology can be used to semantically
enrich RFID systems, and hence, improve their usage and reasoning.
Abstract: This research tested the performance of alternative
warehouse designs concerning the picking process. The chosen
performance measures were Travel Distance and Total Fulfilment
Time. An explanatory case study was built up around a model
implemented with SIMUL8. Hypotheses were set by selecting
outcomes from the literature survey matching popular empirical
findings. 17.4% reductions were found for Total Fulfilment Time and
Resource Utilisation. The latter was then used as a proxy for
operational efficiency. Literal replication of theoretical data-patterns
was considered as an internal validity sign. Assessing the estimated
changes benefits ahead of implementation was found to be a
contribution to practice.
Abstract: Temperature regulating system by gaseous nitrogen is
of importance to the space environment simulator, which keeps the
shrouds in the temperature range from -150°C to +150°C. Liquid
nitrogen spray equipment is one of the most critical parts in the
temperature regulating system by gaseous nitrogen. Y type jet
atomizer and internal mixing atomizer of the liquid nitrogen spray
equipment are studied in this paper, 2D/3D atomizer model was
established and grid division was conducted respectively by the
software of Catia and ICEM. Based on the above preparation,
numerical simulation on the spraying process of the atomizer by
FLUENT is performed. Using air and water as the medium,
comparison between the tests and numerical simulation was conducted
and the results of two ways match well. Hence, it can be conclude that
this atomizer model can be applied in the numerical simulation of
liquid nitrogen spray equipment.
Abstract: In this paper a very simple and effective user
administration view of computing clusters systems is implemented in
order of friendly provide the configuration and monitoring of
distributed application executions. The user view, the administrator
view, and an internal control module create an illusionary
management environment for better system usability. The
architecture, properties, performance, and the comparison with others
software for cluster management are briefly commented.
Abstract: The garment manufacturing industry involves
sequential processes that are subjected to uncontrollable variations.
The industry depends on the skill of labour in handling the varieties
of fabrics and accessories, machines, as well as complicated sewing
operation. Due to these reasons, garment manufacturers have created
systems to monitor and to control the quality of the products on a
regular basis by conducting quality approaches to minimize variation.
With that, the aim of this research has been to ascertain the quality
approaches deployed by Malaysian garment manufacturers in three
key areas - quality systems and tools; quality control and types of
inspection; as well as sampling procedures chosen for garment
inspection. Besides, the focus of this research was to distinguish the
quality approaches adopted by companies that supplied finished
garments to both domestic and international markets. Feedback from
each company representative has been obtained via online survey,
which comprised of five sections and 44 questions on the
organizational profile and the quality approaches employed in the
garment industry. As a result, the response rate was 31%. The results
revealed that almost all companies have established their own
mechanism of process control by conducting a series of quality
inspections for daily production, either it was formally set up or
otherwise. In addition, quality inspection has been the predominant
quality control activity in the garment manufacturing, while the level
of complexity of these activities was substantially dictated by the
customers. Moreover, AQL-based sampling was utilized by
companies dealing with exports, whilst almost all the companies that
only concentrated on the domestic market were comfortable using
their own sampling procedures for garment inspection. Hence, this
research has provided insights into the implementation of a number
of quality approaches that were perceived as important and useful in
the garment manufacturing sector, which is truly labour-intensive.
Abstract: The aim of this study is to empirically investigate the
mediating impact of export performance (EP) between technological
advancement capabilities and business performance (BP) of
Malaysian manufacturing micro, small and medium sized enterprises
(MSME’s). Firm’s technological advancement resources are
hypothesized as a platform to enhance both exports and BP of
manufacturing MSMEs in Malaysia. This study is twofold, primary it
has investigated that technological advancement capabilities helps to
appreciates main performance measures noted in terms of EP and
Secondly, it investigates that how efficiently and effectively
technological advancement capabilities can contribute in overall
Malaysian MSME’s BP. Smart PLS-3 statistical software is used to
know the association between technological advancement
capabilities, MSME’s EP and BP. In this study, the data was
composed from Malaysian manufacturing MSME’s in east coast
industrial zones known as the manufacturing hub of MSMEs. Seven
hundred and fifty (750) questionnaires were distributed, but only 148
usable questionnaires are returned. The finding of this study indicated
that technological advancement capabilities helps to strengthen the
export in term of time and cost efficient and it plays a significant role
in appreciating their BP. This study is helpful for small and medium
enterprise owners who intend to expand their business overseas and
though smart technological advancement resources they can achieve
their business competitiveness and excellence both at local and
international markets.
Abstract: At the present work, highly transparent strip type
quasi-solid state dye-sensitized solar cells (DSSCs) were fabricated
through inkjet printing using nanocomposite TiO2 inks as raw
materials and tested under outdoor illumination conditions. The cells,
which can be considered as the structural units of large area modules,
were fully characterized electrically and electrochemically and after
the evaluation of the received results a large area DSSC module was
manufactured. The module design was a sandwich Z-interconnection
where the working electrode is deposited on one conductive glass and
the counter electrode on a second glass. Silver current collective
fingers were printed on the conductive glasses to make the internal
electrical connections and the adjacent cells were connected in series
and finally insulated using a UV curing resin to protect them from the
corrosive (I-/I3-) redox couple of the electrolyte. Finally, outdoor tests
were carried out to the fabricated dye-sensitized solar module and its
performance data were collected and assessed.
Abstract: Cryosorption pumps are considered safe, quiet, and
ultra-high vacuum production pumps which have their application
from Semiconductor industries to ITER [International Thermonuclear
Experimental Reactor] units. The principle of physisorption of gases
over highly porous materials like activated charcoal at cryogenic
temperatures (below -1500°C) is involved in determining the
pumping speed of gases like Helium, Hydrogen, Argon, and
Nitrogen. This paper aims at providing detailed overview of
development of Cryosorption pump and characterization of different
activated charcoal materials that optimizes the performance of the
pump. Different grades of charcoal were tested in order to determine
the pumping speed of the pump and were compared with
commercially available Varian cryopanel. The results for bare panel,
bare panel with adhesive, cryopanel with pellets, and cryopanel with
granules were obtained and compared. The comparison showed that
cryopanel adhered with small granules gave better pumping speeds
than large sized pellets.
Abstract: Abstract—[Tris (1,10-phenanthroline) lanthanum(III)]
trithiocyanate is a new compound that has shown high ability for
stopping the synthesis of DNA and also acting as a photosensitizer.
Nowadays, the radiation dose assessment resource (RADAR) method
is known as the most common method for absorbed dose calculation.
177Lu was produced by (n, gamma) reaction in a research reactor.
177Lu-PL3 was prepared in the optimized condition. The
radiochemical yield was checked by ITLC method. The
biodistribution of the complex was investigated by intravenously
injection to wild-type rats via their tail veins. In this study, the
absorbed dose of 177Lu-PL3 to human organs was estimated by
RADAR method. 177Lu was prepared with a specific activity of 2.6-3
GBq.mg-1 and radionuclide purity of 99.98 %. Final preparation of
the radiolabelled complex showed high radiochemical purity of >
99%. The results show that liver and spleen have received the highest
absorbed dose of 1.051 and 0.441 mSv/MBq, respectively. The
absorbed dose values for these two dose-limiting tissues suggest
more biological studies special in tumor-bearing animals.
Abstract: The measurement of organ radiation exposure dose is
one of the most important steps to be taken initially, for developing a
new radiopharmaceutical. In this study, the dosimetric studies of a
novel agent for SPECT-imaging of the bone metastasis, 111In-
1,4,7,10-tetraazacyclododecane-1,4,7,10 tetraethylene phosphonic
acid (111In-DOTMP) complex, have been carried out to estimate the
dose in human organs based on the data derived from rats. The
radiolabeled complex was prepared with high radiochemical purity in
the optimal conditions. Biodistribution studies of the complex was
investigated in the male Syrian rats at selected times after injection
(2, 4, 24 and 48 h). The human absorbed dose estimation of the
complex was made based on data derived from the rats by the
radiation absorbed dose assessment resource (RADAR) method.
111In-DOTMP complex was prepared with high radiochemical purity
of >99% (ITLC). Total body effective absorbed dose for 111In-
DOTMP was 0.061 mSv/MBq. This value is comparable to the other
111In clinically used complexes. The results show that the dose with
respect to the critical organs is satisfactory within the acceptable
range for diagnostic nuclear medicine procedures. Generally, 111In-
DOTMP has interesting characteristics and can be considered as a
viable agent for SPECT-imaging of the bone metastasis in the near
future.
Abstract: The last two decades witnessed a movement towards
harmonization of international financial reporting standards (IFRS)
throughout the global economy. This investigation seeks to identify
the factors that could explain the adoption of IFRS by poor
jurisdictions. While there has been a considerable amount of
literature published on the effects and key drivers of IFRS adoption
in both developed and developing countries, little attention has been
paid to jurisdictions with less developed capital markets and low
income levels exclusively. Drawing upon the Institutional Isomorphism theory and analyzing
a sample of 45 poor jurisdictions between 2008 and 2013, the study
empirically shows that poor jurisdictions are driven by legitimacy
concerns rather than by economic reasoning to adopt an international
accounting perspective. This in turn has implications for the IASB, as
it should seek to influence institutional pressures within a particular
jurisdiction in order to promote IFRS adoption.
Abstract: The aim of this study was to determine the factor
structure and psychometric properties (i.e., reliability and convergent
validity) of the Employee Trust Scale, a newly created instrument by
the researchers. The Employee Trust Scale initially contained 82
items to measure employees’ trust toward their supervisors. A sample
of 818 (343 females, 449 males) employees were selected randomly
from public and private organization sectors in Kota Kinabalu,
Sabah, Malaysia. Their ages ranged from 19 to 67 years old with a
mean of 34.55 years old. Their average tenure with their current
employer was 11.2 years (s.d. = 7.5 years). The respondents were
asked to complete the Employee Trust Scale, as well as a managerial
trust questionnaire from Mishra. The exploratory factor analysis on
employees’ trust toward their supervisor’s extracted three factors,
labeled ‘trustworthiness’ (32 items), ‘position status’ (11 items) and
‘relationship’ (6 items) which accounted for 62.49% of the total
variance. Trustworthiness factors were re-categorized into three sub
factors: competency (11 items), benevolence (8 items) and integrity
(13 items). All factors and sub factors of the scales demonstrated
clear reliability with internal consistency of Cronbach’s Alpha above
.85. The convergent validity of the Scale was supported by an
expected pattern of correlations (positive and significant correlation)
between the score of all factors and sub factors of the scale and the
score on the managerial trust questionnaire, which measured the same
construct. The convergent validity of Employee Trust Scale was
further supported by the significant and positive inter-correlation
between the factors and sub factors of the scale. The results suggest
that the Employee Trust Scale is a reliable and valid measure.
However, further studies need to be carried out in other groups of
sample as to further validate the Scale.
Abstract: On account of the concern of the fossil fuel is
depleting and its negative effects on the environment, interest in
alternative energy sources is increasing day by day. However,
considering the importance of transportation in human life, instead of
oil and its derivatives fueled vehicles with internal combustion
engines, electric vehicles which are sensitive to the environment and
working with electrical energy has begun to develop. In this study,
simulation was carried out for providing energy management and
recovering regenerative braking in fuel cell-battery hybrid electric
vehicle. The main power supply of the vehicle is fuel cell on the other
hand not only instantaneous power is supplied by the battery but also
the energy generated due to regenerative breaking is stored in the
battery. Obtained results of the simulation is analyzed and discussed.
Abstract: The present explanatory study concerns with the
relation between Diabetes Mellitus and Food Balance in the Kingdom
of Saudi Arabia during 2005-2010, using published data. Results illustrated that Saudi citizen daily protein consumption
(DPC) during 2005-2007 (g/capita/day) is higher than the average
global consumption level of protein with 15.27%, daily fat
consumption (DFC) with 24.56% and daily energy consumption
(DEC) with 16.93% and increases than recommended level by
International Nutrition Organizations (INO) with 56% for protein,
60.49% for fat and 27.37% for energy. On the other hand, DPC per
capita in Saudi Arabia decreased during the period 2008-2010 from
88.3 to 82.36 gram/ day. Moreover, DFC per capita in Saudi Arabia
decreased during the period 2008-2010 from 3247.90 to 3176.43
Cal/capita/ day, and daily energy consumption (DEC) of Saudi
citizen increases than world consumption with 16.93%, whereas
increases with 27.37% than INO. Despite this, DPC, DFC and DEC
per capita in Saudi Arabia still higher than world mean. On the other
side, results illustrated that the number of diabetic patients in Saudi
Arabia during the same period (2005-2010). The curve of diabetic
patient’s number in Saudi Arabia during 2005-2010 is regular
ascending with increasing level ranged between 7.10% in 2005 and
12.44% in 2010. It is essential to devise Saudi National programs to educate the
public about the relation of food balances and diabetes so it could be
avoided, and provide citizens with healthy dietary balances tables.
Abstract: Cloud Computing refers to applications delivered as
services over the internet, and the datacenters that provide those
services with hardware and systems software. These were earlier
referred to as Software as a Service (SaaS). Scheduling is justified by
job components (called tasks), lack of information. In fact, in a large
fraction of jobs from machine learning, bio-computing, and image
processing domains, it is possible to estimate the maximum time
required for a task in the job. This study focuses on Trust based
scheduling to improve cloud security by modifying Heterogeneous
Earliest Finish Time (HEFT) algorithm. It also proposes TR-HEFT
(Trust Reputation HEFT) which is then compared to Dynamic Load
Scheduling.
Abstract: Recently, numerous documents including large
volumes of unstructured data and text have been created because of the
rapid increase in the use of social media and the Internet. Usually,
these documents are categorized for the convenience of users. Because
the accuracy of manual categorization is not guaranteed, and such
categorization requires a large amount of time and incurs huge costs.
Many studies on automatic categorization have been conducted to help
mitigate the limitations of manual categorization. Unfortunately, most
of these methods cannot be applied to categorize complex documents
with multiple topics because they work on the assumption that
individual documents can be categorized into single categories only.
Therefore, to overcome this limitation, some studies have attempted to
categorize each document into multiple categories. However, the
learning process employed in these studies involves training using a
multi-categorized document set. These methods therefore cannot be
applied to the multi-categorization of most documents unless
multi-categorized training sets using traditional multi-categorization
algorithms are provided. To overcome this limitation, in this study, we
review our novel methodology for extending the category of a
single-categorized document to multiple categorizes, and then
introduce a survey-based verification scenario for estimating the
accuracy of our automatic categorization methodology.