Abstract: Syringe pumps are commonly used for drug delivery in hospitals and clinical environments. These instruments are critical in neonatology and oncology, where any variation in the flow rate and drug dosing quantity can lead to severe incidents and even death of the patient. Therefore it is very important to determine the accuracy and precision of these devices using the suitable calibration methods. The Volume Laboratory of the Portuguese Institute for Quality (LVC/IPQ) uses two different methods to calibrate syringe pumps from 16 nL/min up to 20 mL/min. The Interferometric method uses an interferometer to monitor the distance travelled by a pusher block of the syringe pump in order to determine the flow rate. Therefore, knowing the internal diameter of the syringe with very high precision, the travelled distance, and the time needed for that travelled distance, it was possible to calculate the flow rate of the fluid inside the syringe and its uncertainty. As an alternative to the gravimetric and the interferometric method, a methodology based on the application of optical technology was also developed to measure flow rates. Mainly this method relies on measuring the increase of volume of a drop over time. The objective of this work is to compare the results of the calibration of two syringe pumps using the different methodologies described above. The obtained results were consistent for the three methods used. The uncertainties values were very similar for all the three methods, being higher for the optical drop method due to setup limitations.
Abstract: Confocal spectral interferometry (CSI) is an innovative optical method for determining microtopography of surfaces and thickness of transparent layers, based on the combination of two optical principles: confocal imaging, and spectral interferometry. Confocal optical system images at each instant a single point of the sample. The whole surface is reconstructed by plan scanning. The interference signal generated by mixing two white-light beams is analyzed using a spectrometer. In this work, five ‘rugotests’ of known standard roughnesses are investigated. The topography is then measured and illustrated, and the equivalent roughness is determined and compared with the standard values.
Abstract: Ellipsometry is an optical method based on the study of the behavior of polarized light. The light reflected on a surface induces a change in the polarization state which depends on the characteristics of the material (complex refractive index and thickness of the different layers constituting the device). The purpose of this work is to determine the optical properties of semiconductor thin films by ellipsometry. This paper describes the experimental aspects concerning the semiconductor samples, the SE400 ellipsometer principle, and the results obtained by direct measurements of ellipsometric parameters and modelling using appropriate software.
Abstract: The laser-ultrasonic method is realized for
quantifying the influence of porosity on the local Young’s
modulus of isotropic composite materials. The method is based on
a laser thermooptical method of ultrasound generation combined
with measurement of the phase velocity of longitudinal and shear
acoustic waves in samples. The main advantage of this method
compared with traditional ultrasonic research methods is the
efficient generation of short and powerful probing acoustic pulses
required for reliable testing of ultrasound absorbing and
scattering heterogeneous materials. Using as an example samples
of a metal matrix composite with reinforcing microparticles of
silicon carbide in various concentrations, it is shown that to
provide an effective increase in Young’s modulus with increasing
concentration of microparticles, the porosity of the final sample
should not exceed 2%.
Abstract: Computer aided design accounts with the support of
parametric software in the design of machine components as well as
of any other pieces of interest. The complexities of the element under
study sometimes offer certain difficulties to computer design, or ever
might generate mistakes in the final body conception. Reverse
engineering techniques are based on the transformation of already
conceived body images into a matrix of points which can be
visualized by the design software. The literature exhibits several
techniques to obtain machine components dimensional fields, as
contact instrument (MMC), calipers and optical methods as laser
scanner, holograms as well as moiré methods. The objective of this
research work was to analyze the moiré technique as instrument of
reverse engineering, applied to bodies of nom complex geometry as
simple solid figures, creating matrices of points. These matrices were
forwarded to a parametric software named SolidWorks to generate
the virtual object. Volume data obtained by mechanical means, i.e.,
by caliper, the volume obtained through the moiré method and the
volume generated by the SolidWorks software were compared and
found to be in close agreement. This research work suggests the
application of phase shifting moiré methods as instrument of reverse
engineering, serving also to support farm machinery element designs.
Abstract: The dynamical contouring error is a critical element for the accuracy of machine tools. The contouring error is defined as the difference between the processing actual path and commanded path, which is implemented by following the command curves from feeding driving system in machine tools. The contouring error is resulted from various factors, such as the external loads, friction, inertia moment, feed rate, speed control, servo control, and etc. Thus, the study proposes a 2D compensating system for the contouring accuracy of machine tools. Optical method is adopted by using stable frequency laser diode and the high precision position sensor detector (PSD) to performno-contact measurement. Results show the related accuracy of position sensor detector (PSD) of 2D contouring accuracy compensating system was ±1.5 μm for a calculated range of ±3 mm, and improvement accuracy is over 80% at high-speed feed rate.
Abstract: The presented paper shows the possibility of using
holographic interferometry for measurement of temperature field in
moving fluids. There are a few methods for identification of velocity
fields in fluids, such us LDA, PIV, hot wire anemometry. It is very
difficult to measure the temperature field in moving fluids. One of the
often used methods is Constant Current Anemometry (CCA), which
is a point temperature measurement method. Data are possibly
acquired at frequencies up to 1000Hz. This frequency should be
limiting factor for using of CCA in fluid when fast change of
temperature occurs. This shortcoming of CCA measurements should
be overcome by using of optical methods such as holographic
interferometry. It is necessary to employ a special holographic setup
with double sensitivity instead of the commonly used Mach-Zehnder
type of holographic interferometer in order to attain the parameters
sufficient for the studied case. This setup is not light efficient like the
Mach-Zehnder type but has double sensitivity. The special technique
of acquiring and phase averaging of results from holographic
interferometry is also presented. The results from the holographic
interferometry experiments will be compared with the temperature
field achieved by methods CCA method.
Abstract: Application of wood in rural construction is diffused
all around the world since remote times. However, its inclusion in
structural design deserves strong support from broad knowledge of
material properties. The pertinent literature reveals the application of
optical methods in determining the complete field displacement on
bodies exhibiting regular as well as irregular surfaces. The use of
moiré techniques in experimental mechanics consists in analyzing the
patterns generated on the body surface before and after deformation.
The objective of this research work is to study the qualitative
deformation behavior of wooden testing specimens under specific
loading situations. The experiment setup follows the literature
description of shadow moiré methods. Results indicate strong
anisotropy influence of the generated displacement field. Important
qualitative as well as quantitative stress and strain distribution were
obtained wooden members which are applicable to rural
constructions.