Abstract: Single crystals of Magnesium alloys such as pure Mg,
Mg-1Zn-0.5Y, Mg-0.1Y, and Mg-0.1Ce alloys were successfully
fabricated in this study by employing the modified Bridgman method.
To determine the exact orientation of crystals, pole figure
measurement using X-ray diffraction were carried out on each single
crystal. Hardness and compression tests were conducted followed by
subsequent recrysatllization annealing. Recrystallization kinetics of
Mg alloy single crystals has been investigated. Fabricated single
crystals were cut into rectangular shaped specimen and solution
treated at 400oC for 24 hrs, and then deformed in compression mode
by 30% reduction. Annealing treatment for recrystallization has been
conducted on these cold-rolled plates at temperatures of 300oC for
various times from 1 to 20 mins. The microstructure observation and
hardness measurement conducted on the recrystallized specimens
revealed that static recrystallization of ternary alloy single crystal was
very slow, while recrystallization behavior of binary alloy single
crystals appeared to be very fast.
Abstract: Single crystals of Magnesium alloys such as Mg-1Al,
Mg-1Zn-0.5Y, Mg-3Li, and AZ31 alloys were successfully fabricated in this study by employing the modified Bridgman method. Single
crystals of pure Mg were also made in this study. To determine the exact orientation of crystals, Laue back-reflection method and pole figure measurement were carried out on each single crystal. Dimensions of single crystals were 10 mm in diameter and 120 mm in
length. Hardness and compression tests were conducted and the results
revealed that hardness and the strength strongly depended on the
orientation. The closer to basal one the orientation was, the higher hardness and compressive strength were. The effect of alloying was
not higher than that of orientation. After compressive deformation of single crystals, the orientation of the crystals was found to rotate and to be parallel to the basal orientation.