Abstract: The present study is aimed at investigating microhardness and density of aluminium alloy chips when subjected to various settings of preheating temperature and preheating time. Three values of preheating temperature were taken as 450 °C, 500 °C, and 550 °C. On the other hand, three values of preheating time were chosen (1, 2, 3) hours. The influences of the process parameters (preheating temperature and time) were analyzed using Design of Experiments (DOE) approach whereby full factorial design with center point analysis was adopted. The total runs were 11 and they comprise of two factors of full factorial design with 3 center points. The responses were microhardness and density. The results showed that the density and microhardness increased with decreasing the preheating temperature. The results also found that the preheating temperature is more important to be controlled rather than the preheating time in microhardness analysis while both the preheating temperature and preheating time are important in density analysis. It can be concluded that setting temperature at 450 °C for 1 hour resulted in the optimum responses.
Abstract: A factorial design of experiments and a response surface methodology were implemented to investigate the liquid-liquid extraction process of zinc (II) from acetate medium using the 1-Butyl-imidazolium di(2-ethylhexyl) phosphate [BIm+][D2EHP-]. The optimization process of extraction parameters such as the initial pH effect (2.5, 4.5, and 6.6), ionic liquid concentration (1, 5.5, and 10 mM) and salt effect (0.01, 5, and 10 mM) was carried out using a three-level full factorial design (33). The results of the factorial design demonstrate that all these factors are statistically significant, including the square effects of pH and ionic liquid concentration. The results showed that the order of significance: IL concentration > salt effect > initial pH. Analysis of variance (ANOVA) showing high coefficient of determination (R2 = 0.91) and low probability values (P < 0.05) signifies the validity of the predicted second-order quadratic model for Zn (II) extraction. The optimum conditions for the extraction of zinc (II) at the constant temperature (20 °C), initial Zn (II) concentration (1mM) and A/O ratio of unity were: initial pH (4.8), extractant concentration (9.9 mM), and NaCl concentration (8.2 mM). At the optimized condition, the metal ion could be quantitatively extracted.
Abstract: Textile industries cater to varied customer preferences and contribute substantially to the economy. However, these textile industries also produce a considerable amount of effluents. Prominent among these are the azo dyes which impart considerable color and toxicity even at low concentrations. Azo dyes are also used as coloring agents in food and pharmaceutical industry. Despite their applications, azo dyes are also notorious pollutants and carcinogens. Popular techniques like photo-degradation, biodegradation and the use of oxidizing agents are not applicable for all kinds of dyes, as most of them are stable to these techniques. Chemical coagulation produces a large amount of toxic sludge which is undesirable and is also ineffective towards a number of dyes. Most of the azo dyes are stable to UV-visible light irradiation and may even resist aerobic degradation. Adsorption has been the most preferred technique owing to its less cost, high capacity and process efficiency and the possibility of regenerating and recycling the adsorbent. Adsorption is also most preferred because it may produce high quality of the treated effluent and it is able to remove different kinds of dyes. However, the adsorption process is influenced by many variables whose inter-dependence makes it difficult to identify optimum conditions. The variables include stirring speed, temperature, initial concentration and adsorbent dosage. Further, the internal diffusional resistance inside the adsorbent particle leads to slow uptake of the solute within the adsorbent. Hence, it is necessary to identify optimum conditions that lead to high capacity and uptake rate of these pollutants. In this work, commercially available activated carbon was chosen as the adsorbent owing to its high surface area. A typical azo dye found in textile effluent waters, viz. the monoazo Acid Orange 10 dye (CAS: 1936-15-8) has been chosen as the representative pollutant. Adsorption studies were mainly focused at obtaining equilibrium and kinetic data for the batch adsorption process at different process conditions. Studies were conducted at different stirring speed, temperature, adsorbent dosage and initial dye concentration settings. The Full Factorial Design was the chosen statistical design framework for carrying out the experiments and identifying the important factors and their interactions. The optimum conditions identified from the experimental model were validated with actual experiments at the recommended settings. The equilibrium and kinetic data obtained were fitted to different models and the model parameters were estimated. This gives more details about the nature of adsorption taking place. Critical data required to design batch adsorption systems for removal of Acid Orange 10 dye and identification of factors that critically influence the separation efficiency are the key outcomes from this research.
Abstract: There is not much effective guideline on development of design parameters selection on spring back for advanced high strength steel sheet metal in U-channel process during cold forming process. This paper presents the development of predictive model for spring back in U-channel process on advanced high strength steel sheet employing Response Surface Methodology (RSM). The experimental was performed on dual phase steel sheet, DP590 in Uchannel forming process while design of experiment (DoE) approach was used to investigates the effects of four factors namely blank holder force (BHF), clearance (C) and punch travel (Tp) and rolling direction (R) were used as input parameters using two level values by applying Full Factorial design (24 ). From a statistical analysis of variant (ANOVA), result showed that blank holder force (BHF), clearance (C) and punch travel (Tp) displayed significant effect on spring back of flange angle (β2 ) and wall opening angle (β1 ), while rolling direction (R) factor is insignificant. The significant parameters are optimized in order to reduce the spring back behavior using Central Composite Design (CCD) in RSM and the optimum parameters were determined. A regression model for spring back was developed. The effect of individual parameters and their response was also evaluated. The results obtained from optimum model are in agreement with the experimental values.
Abstract: The quality of video transmitted by mobile ad hoc networks (MANETs) can be influenced by several factors, including protocol layers; parameter settings of each protocol. In this paper, we are concerned with understanding the functional relationship between these influential factors and objective video quality in MANETs. We illustrate a systematic statistical design of experiments (DOE) strategy can be used to analyze MANET parameters and performance. Using a 2k factorial design, we quantify the main and interactive effects of 7 factors on a response metric (i.e., mean opinion score (MOS) calculated by PSNR with Evalvid package) we then develop a first-order linear regression model between the influential factors and the performance metric.
Abstract: The development of biomimetic micro-aerial-vehicles
(MAVs) with flapping wings is the future trend in military/domestic
field. The successful flight of MAVs is strongly related to the
understanding of unsteady aerodynamic performance of low Reynolds
number airfoils under dynamic flapping motion. This study explored
the effects of flapping frequency, stroke amplitude, and the inclined
angle of stroke plane on lift force and thrust force of a bio-inspiration
corrugated airfoil with 33 full factorial design of experiment and
ANOVA analysis. Unsteady vorticity flows over a corrugated thin
airfoil executing flapping motion are computed with time-dependent
two-dimensional laminar incompressible Reynolds-averaged
Navier-Stokes equations with the conformal hybrid mesh. The tested
freestream Reynolds number based on the chord length of airfoil as
characteristic length is fixed of 103. The dynamic mesh technique is
applied to model the flapping motion of a corrugated airfoil. Instant
vorticity contours over a complete flapping cycle clearly reveals the
flow mechanisms for lift force generation are dynamic stall, rotational
circulation, and wake capture. The thrust force is produced as the
leading edge vortex shedding from the trailing edge of airfoil to form a
reverse von Karman vortex. Results also indicated that the inclined
angle is the most significant factor on both the lift force and thrust
force. There are strong interactions between tested factors which mean
an optimization study on parameters should be conducted in further
runs.
Abstract: The objective of this research is parameters optimized
of the stair shape workpiece which is cut by CNC Wire-Cut EDM
(WEDW). The experiment material is SKD-11 steel of stair-shaped
with variable height workpiece 10, 20, 30 and 40 mm. with the same
10 mm. thickness are cut by Sodick's CNC Wire-Cut EDM model
AD325L.
The experiments are designed by 3k full factorial experimental
design at 3 level 2 factors and 9 experiments with 2 replicate. The
selected two factor are servo voltage (SV) and servo feed rate (SF)
and the response is cutting thickness error. The experiment is divided
in two experiments. The first experiment determines the significant
effective factor at confidential interval 95%. The SV factor is the
significant effective factor from first result. In order to result smallest
cutting thickness error of workpieces is 17 micron with the SV value
is 46 volt. Also show that the lower SV value, the smaller different
thickness error of workpiece. Then the second experiment is done to
reduce different cutting thickness error of workpiece as small as
possible by lower SV. The second experiment result show the
significant effective factor at confidential interval 95% is the SV
factor and the smallest cutting thickness error of workpieces reduce
to 11 micron with the experiment SV value is 36 volt.
Abstract: The use of electronic sensors in the electronics
industry has become increasingly popular over the past few years,
and it has become a high competition product. The frequency
adjustment process is regarded as one of the most important process
in the electronic sensor manufacturing process. Due to inaccuracies
in the frequency adjustment process, up to 80% waste can be caused
due to rework processes; therefore, this study aims to provide a
preliminary understanding of the role of parameters used in the
frequency adjustment process, and also make suggestions in order to
further improve performance. Four parameters are considered in this
study: air pressure, dispensing time, vacuum force, and the distance
between the needle tip and the product. A full factorial design for
experiment 2k was considered to determine those parameters that
significantly affect the accuracy of the frequency adjustment process,
where a deviation in the frequency after adjustment and the target
frequency is expected to be 0 kHz. The experiment was conducted on
two levels, using two replications and with five center-points added.
In total, 37 experiments were carried out. The results reveal that air
pressure and dispensing time significantly affect the frequency
adjustment process. The mathematical relationship between these
two parameters was formulated, and the optimal parameters for air
pressure and dispensing time were found to be 0.45 MPa and 458 ms,
respectively. The optimal parameters were examined by carrying out
a confirmation experiment in which an average deviation of 0.082
kHz was achieved.
Abstract: Development of artificial neural network (ANN) for
prediction of aluminum workpieces' surface roughness in ultrasonicvibration
assisted turning (UAT) has been the subject of the present
study. Tool wear as the main cause of surface roughness was also
investigated. ANN was trained through experimental data obtained
on the basis of full factorial design of experiments. Various
influential machining parameters were taken into consideration. It
was illustrated that a multilayer perceptron neural network could
efficiently model the surface roughness as the response of the
network, with an error less than ten percent. The performance of the
trained network was verified by further experiments. The results of
UAT were compared with the results of conventional turning
experiments carried out with similar machining parameters except for
the vibration amplitude whence considerable reduction was observed
in the built-up edge and the surface roughness.