Abstract: Effect of Zn addition on the microstructure and
mechanical properties of Mg-Zn alloys with Zn contents from 6 to 10
weight percent was investigated in this study. Through calculation of
phase equilibria of Mg-Zn alloys, carried out by using FactSage® and
FTLite database, solution treatment temperature was decided as
temperatures from 300 to 400oC, where supersaturated solid solution
can be obtained. Solid solution treatment of Mg-Zn alloys was
successfully conducted at 380oC and supersaturated microstructure
with all beta phase resolved into matrix was obtained. After solution
treatment, hot rolling was successfully conducted by reduction of
60%. Compression and tension tests were carried out at room
temperature on the samples as-cast, solution treated, hot-rolled and
recrystallized after rolling. After solid solution treatment, each alloy
was annealed at temperatures of 180 and 200oC for time intervals from
1 min to 48 hrs and hardness of each condition was measured by
micro-Vickers method. Peak aging conditions were deduced as at the
temperature of 200oC for 10 hrs. By addition of Zn by 10 weight
percent, hardness and strength were enhanced.
Abstract: Effect of alloying on the microstructure and mechanical properties of heat-resisting duplex stainless steel (DSS) for Mg production was investigated in this study. 25Cr-8Ni based DSS’s were cast into rectangular ingots of which the dimension was 350×350×100 mm3 . Nitrogen and Yttrium were added in the range within 0.3 in weight percent. Phase equilibrium was calculated using the FactSage®, thermodynamic software. Hot exposure, high temperature tensile and compression tests were conducted on the ingots at 1230oC, which is operation temperature employed for Mg production by Silico-thermic reduction. The steel with N and Y showed much higher strength than 310S alloy in both tensile and compression tests. By thermal exposition at 1230oC for 200 hrs, hardness of DSS containing N and Y was found to increase. Hot workability of the heat-resisting DSS was evaluated by employing hot rolling at 1230 oC. Hot shortness was observed in the ingot with N and found to disappear after addition of Y.
Abstract: Phase equilibria of AZ91D Mg alloys for
nonflammable use, containing Ca and Y, were carried out by using
FactSage® and FTLite database, which revealed that solid solution
treatment could be performed at temperatures from 400 to 450oC.
Solid solution treatment of AZ91D Mg alloy without Ca and Y was
successfully conducted at 420oC and supersaturated microstructure
with all beta phase resolved into matrix was obtained. In the case of
AZ91D Mg alloy with some Ca and Y; however, a little amount of
intermetallic particles were observed after solid solution treatment.
After solid solution treatment, each alloy was annealed at temperatures
of 180 and 200oC for time intervals from 1 min to 48 hrs and hardness
of each condition was measured by micro-Vickers method. Peak aging
conditions were deduced as at the temperature of 200oC for 10 hrs.
Abstract: High temperature deformation behavior of cast
Fe-20Cr-5Al alloy has been investigated in this study by performing
tensile and compression tests at temperatures from 1100 to 1200oC.
Rectangular ingots of which the dimensions were 300×300×100 in
millimeter were cast using vacuum induction melting. Phase
equilibrium was calculated using the FactSage®, thermodynamic
software and database. Tensile strength of cast Fe-20Cr-5Al alloy was
4 MPa at 1200oC. With temperature decreased, tensile strength
increased rapidly and reached up to 13 MPa at 1100oC. Elongation
also increased from 18 to 80% with temperature decreased from
1200oC to 1100oC. Microstructure observation revealed that M23C6
carbide was precipitated along the grain boundary and within the
matrix.
Abstract: High temperature deformation behavior of cast 310S stainless steel has been investigated in this study by performing tensile and compression tests at temperatures from 900 to 1200oC. Rectangular ingots of which the dimensions were 350×350×100 in millimeter were cast using vacuum induction melting. Phase equilibrium was calculated using the FactSage®, thermodynamic software and database. Thermal expansion coefficient was also measured on the ingot in the temperature range from room temperature to 1200oC. Tensile strength of cast 310S stainless steel was 9 MPa at 1200oC, which is a little higher than that of a wrought 310S. With temperature decreased, tensile strength increased rapidly and reached up to 72 MPa at 900oC. Elongation also increased with temperature decreased. Microstructure observation revealed that s phase was precipitated along the grain boundary and within the matrix over 1200oC, which is detrimental to high temperature elongation.
Abstract: The effect of Yttrium addition on the microstructure and mechanical properties of Sn-Zn eutectic alloy, which has been attracting intensive focus as a Pb-free solder material, was investigated in this study. Phase equilibrium has been calculated by using FactSage® to evaluate the composition and fraction of equilibrium intermetallic compounds and construct a phase diagram. In the case of Sn-8.8Zn eutectic alloy, the as-cast microstructure was typical lamellar. With addition of 0.25wt.%Y, a large amount of pro-eutectic a phase have been observed and various YZnx intermetallic compounds were expected to successively form during cooling. Hardness of Sn-8.8Zn alloy was not affected by Y-addition and both alloys could be rolled by 90% at room temperature.
Abstract: Most buildings have been using anchor bolts
commonly for installing outdoor advertising structures. Anchor bolts
of common carbon steel are widely used and often installed
indiscriminately by inadequate installation standards. In the area
where strong winds frequently blow, falling accidents of outdoor
advertising structures can occur and cause a serious disaster, which is
very dangerous and to be prevented. In this regard, the development of
high-performance anchor bolts is urgently required. In the present
study, 25Cr-8Ni-1.5Si-1Mn-0.4C alloy was produced by traditional
vacuum induction melting (VIM) for the application of anchor bolt.
The alloy composition is revealed as a duplex microstructure from
thermodynamic phase analysis by FactSage® and confirmed by
metallographic experiment. Addition of Nitrogen to the alloy was
found to reduce the ferritic phase domain and significantly increase the
hardness and the tensile strength. Microstructure observation revealed
mixed structure of austenite and ferrite with fine carbide distributed
along the grain and phase boundaries.