Abstract: The mechanism for extraction bioactive compounds
from plant matrix is essential for optimizing the extraction process. As
a benchmark technique, a soxhlet extraction has been utilized for
discussing the mechanism and compared with an accelerated water
extraction. The trends of both techniques show that the process
involves extraction and degradation. The highest yields of 6-, 8-,
10-gingerols and 6-shogaol in soxhlet extraction were 13.948, 7.12,
10.312 and 2.306 mg/g, respectively. The optimum 6-, 8-,
10-gingerols and 6-shogaol extracted by the accelerated water
extraction at 140oC were 68.97±3.95 mg/g at 3min, 18.98±3.04 mg/g
at 5min, 5.167±2.35 mg/g at 3min and 14.57±6.27 mg/g at 3min,
respectively. The effect of temperature at 3mins shows that the
concentration of 6-shogaol increased rapidly as decreasing the
recovery of 6-gingerol.
Abstract: Horseradish (Armoracia rusticana) is a perennial herb belonging to the Brassicaceae family and contains biologically active substances. The aim of the current research was to determine best method for extraction of phenolic compounds from horseradish roots showing high antiradical activity. Three genotypes (No. 105; No. 106 and variety ‘Turku’) of horseradish roots were extracted with eight different solvents: n-hexane, ethyl acetate, diethyl ether, 2-propanol, acetone, ethanol (95%), ethanol / water / acetic acid (80/20/1 v/v/v) and ethanol / water (80/20 by volume) using two extraction methods (conventional and Soxhlet). As the best solvents ethanol and ethanol / water solutions can be chosen. Although in Soxhlet extracts TPC was higher, scavenging activity of DPPH˙ radicals did not increase. It can be concluded that using Soxhlet extraction method more compounds that are not effective antioxidants.
Abstract: Subcritical water extraction was investigated as a
novel and alternative technology in the food and pharmaceutical
industry for the separation of Mannitol from olive leaves and its
results was compared with those of Soxhlet extraction. The effects of
temperature, pressure, and flow rate of water and also momentum
and mass transfer dimensionless variables such as Reynolds and
Peclet Numbers on extraction yield and equilibrium partition
coefficient were investigated. The 30-110 bars, 60-150°C, and flow
rates of 0.2-2 mL/min were the water operating conditions. The
results revealed that the highest Mannitol yield was obtained at
100°C and 50 bars. However, extraction of Mannitol was not
influenced by the variations of flow rate. The mathematical modeling
of experimental measurements was also investigated and the model is
capable of predicting the experimental measurements very well. In
addition, the results indicated higher extraction yield for the
subcritical water extraction in contrast to Soxhlet method.