Accelerated Microwave Extraction of Natural Product using the Cryogrinding
Team distillation assisted by microwave extraction
(SDAM) considered as accelerated technique extraction is a
combination of microwave heating and steam distillation, performed
at atmospheric pressure. SDAM has been compared with the same
technique coupled with the cryogrinding of seeds (SDAM -CG).
Isolation and concentration of volatile compounds are performed by a
single stage for the extraction of essential oil from Cuminum
cyminum seeds. The essential oils extracted by these two methods for
5 min were quantitatively (yield) and qualitatively (aromatic profile)
no similar. These methods yield an essential oil with higher amounts
of more valuable oxygenated compounds, and allow substantial
savings of costs, in terms of time, energy and plant material. SDAM
and SDAM-CG is a green technology and appears as a good
alternative for the extraction of essential oils from aromatic plants.
[1] S.Behera, S. Nagarajan,, J.M.L.Rao, Microwave heating and
conventional roasting of cuminseeds (Cuminum cyminum L.) and
effect on chemical composition ofvolatiles.Food Chem.87, pp.25-
29.2004.
[2] K. Uma Pradeep, P.Geervani,, B.O. Eggum, B.O.Common Indian spices:
nutrient composition, consumption and contribution to dietary value.
Plant Foods Hum. Nutr. 44 (2), pp.137-148? 1993
[3] The Wealth of India, A Dictionary of Indian Raw Materials & Industrial
Products, Vol. 2. CSIR, New Delhi, pp. 257, 2001
[4] M.P. Lompart, R.A. Lorenzo, Cela, R.,1997, Optimization of a
Microwave assisted Extraction Method for Phenol and Methylphenol
Isomers in Soil Samples Using a Central Composite DesignParé,
J.R.J. Analyst, 122, pp.133-137,1997.
[5] F. Benkaci-Ali, A. Baaliouamer, B.Y. Meklati, Etude comparative de la
composition chimique de la Nigella sativa de quelques régions du
monde, extraite par micro-ondes Rivista Italiana EPPOS, 40, pp.15-
24,2005.
[6] M.E. Lucchesi, F. Chemat, J. Smadja, Solvent-free microwave
extraction of essential oil from aromatic herbs: comparison with
conventional hydrodistillation, J. Chromatogr. A, 1043, pp.323-327,
2004.
[7] J.R.J. Paré, J.M.R. Belanger, S.S. Stafford, A new tool for the analytical
laboratory , Trends in Analytical Chemistry Trends Anal.Chem.13,
pp.176-184, 1994
[8] F. Benkaci-AlI, A. BaaliouameR, B.Y. Meklati, Kinetic Study of
Microwave Extraction of Essential Oil of Nigella sativa L. Seeds,
Chromatographia, vol. 64, 3-4, pp.227-231,2006.
[9] Conseil de l-Europe, Pharmacopée Européenne 1, Maisonneuve S.A.
Editions, Sainte Ruffine, 1996.
[10] R.P. Adams, Identification of essential oil components by gas
chromatography/mass spectroscopy. 4th edition. Allured Publishing
Corporation, Carol Stream. 2007
[11] Jae Hun Kim, J.H. Mee-Hye Shin, Young-Jeong Hwang, Periasamy
Srinivasan a, JaeK yung Kim, Hyun Jin Park e, MyungWooByun a,
JuWoonLe, Role of gamma irradiation on the natural antioxidants in
cumin seeds Radiation Physics and Chemistry 78,pp.153-157, 2009.
[12] M. Jalali-Heravi, B. Zekavat, H. Sereshti, Use of gas chromatography-
mass spectrometry combined with resolution methods to characterize the
essential oil components of Iranian cumin and caraway, J. Chromatogr.
A, 1143, pp.215-226, 2007.
[1] S.Behera, S. Nagarajan,, J.M.L.Rao, Microwave heating and
conventional roasting of cuminseeds (Cuminum cyminum L.) and
effect on chemical composition ofvolatiles.Food Chem.87, pp.25-
29.2004.
[2] K. Uma Pradeep, P.Geervani,, B.O. Eggum, B.O.Common Indian spices:
nutrient composition, consumption and contribution to dietary value.
Plant Foods Hum. Nutr. 44 (2), pp.137-148? 1993
[3] The Wealth of India, A Dictionary of Indian Raw Materials & Industrial
Products, Vol. 2. CSIR, New Delhi, pp. 257, 2001
[4] M.P. Lompart, R.A. Lorenzo, Cela, R.,1997, Optimization of a
Microwave assisted Extraction Method for Phenol and Methylphenol
Isomers in Soil Samples Using a Central Composite DesignParé,
J.R.J. Analyst, 122, pp.133-137,1997.
[5] F. Benkaci-Ali, A. Baaliouamer, B.Y. Meklati, Etude comparative de la
composition chimique de la Nigella sativa de quelques régions du
monde, extraite par micro-ondes Rivista Italiana EPPOS, 40, pp.15-
24,2005.
[6] M.E. Lucchesi, F. Chemat, J. Smadja, Solvent-free microwave
extraction of essential oil from aromatic herbs: comparison with
conventional hydrodistillation, J. Chromatogr. A, 1043, pp.323-327,
2004.
[7] J.R.J. Paré, J.M.R. Belanger, S.S. Stafford, A new tool for the analytical
laboratory , Trends in Analytical Chemistry Trends Anal.Chem.13,
pp.176-184, 1994
[8] F. Benkaci-AlI, A. BaaliouameR, B.Y. Meklati, Kinetic Study of
Microwave Extraction of Essential Oil of Nigella sativa L. Seeds,
Chromatographia, vol. 64, 3-4, pp.227-231,2006.
[9] Conseil de l-Europe, Pharmacopée Européenne 1, Maisonneuve S.A.
Editions, Sainte Ruffine, 1996.
[10] R.P. Adams, Identification of essential oil components by gas
chromatography/mass spectroscopy. 4th edition. Allured Publishing
Corporation, Carol Stream. 2007
[11] Jae Hun Kim, J.H. Mee-Hye Shin, Young-Jeong Hwang, Periasamy
Srinivasan a, JaeK yung Kim, Hyun Jin Park e, MyungWooByun a,
JuWoonLe, Role of gamma irradiation on the natural antioxidants in
cumin seeds Radiation Physics and Chemistry 78,pp.153-157, 2009.
[12] M. Jalali-Heravi, B. Zekavat, H. Sereshti, Use of gas chromatography-
mass spectrometry combined with resolution methods to characterize the
essential oil components of Iranian cumin and caraway, J. Chromatogr.
A, 1143, pp.215-226, 2007.
@article{"International Journal of Chemical, Materials and Biomolecular Sciences:53686", author = "F. Benkaci-Ali and R. Mekaoui and G. Eppe and E. De Pau and J. F. Faucont", title = "Accelerated Microwave Extraction of Natural Product using the Cryogrinding", abstract = "Team distillation assisted by microwave extraction
(SDAM) considered as accelerated technique extraction is a
combination of microwave heating and steam distillation, performed
at atmospheric pressure. SDAM has been compared with the same
technique coupled with the cryogrinding of seeds (SDAM -CG).
Isolation and concentration of volatile compounds are performed by a
single stage for the extraction of essential oil from Cuminum
cyminum seeds. The essential oils extracted by these two methods for
5 min were quantitatively (yield) and qualitatively (aromatic profile)
no similar. These methods yield an essential oil with higher amounts
of more valuable oxygenated compounds, and allow substantial
savings of costs, in terms of time, energy and plant material. SDAM
and SDAM-CG is a green technology and appears as a good
alternative for the extraction of essential oils from aromatic plants.", keywords = "Steam distillation, microwave extraction, Cuminum
cyminum, chromatography, mass spectrometry", volume = "6", number = "8", pages = "703-4", }