Abstract: This work aims to investigate the structure–property
relationship in ternary nanocomposites consisting of polypropylene
as the matrix, polyamide 66 as the minor phase and treated nanoclay
DELLITE 67G as the reinforcement. All PP/PA66/Nanoclay systems
with polypropylene grafted maleic anhydride PP-g-MAH as a
compatibilizer were prepared via melt compounding and
characterized in terms of nanoclay content. Morphological structure
was investigated by scanning electron microscopy. The rheological
behavior of the nanocomposites was determined by various methods,
viz melt flow index (MFI) and parallel plate rheological
measurements. The PP/PP-g-MAH/PA66 nanocomposites showed a homogeneous
morphology supporting the compatibility improvement between PP,
PA66, and nanoclay. SEM results revealed the formation of
nanocomposites as the nanoclay was intercalated and exfoliated. In
the ternary nanocomposites, the rheological behavior showed that, the
complex viscosity is increased with increasing the nanoclay. The results showed that the use of nanoclay affects the variations
of storage modulus (G′), loss modulus (G″) and the melt elasticity.
Abstract: This study was aimed to measure effective transverse
relaxation rates (R2*) in the liver and muscle of normal New Zealand
White (NZW) rabbits. R2* relaxation rate has been widely used in
various hepatic diseases for iron overload by quantifying iron contents
in liver. R2* relaxation rate is defined as the reciprocal of T2*
relaxation time and mainly depends on the constituents of tissue.
Different tissues would have different R2* relaxation rates. The signal
intensity decay in Magnetic resonance imaging (MRI) may be
characterized by R2* relaxation rates. In this study, a 1.5T GE Signa
HDxt whole body MR scanner equipped with an 8-channel high
resolution knee coil was used to observe R2* values in NZW rabbit’s
liver and muscle. Eight healthy NZW rabbits weighted 2 ~ 2.5 kg were
recruited. After anesthesia using Zoletil 50 and Rompun 2% mixture,
the abdomen of rabbit was landmarked at the center of knee coil to
perform 3-plane localizer scan using fast spoiled gradient echo
(FSPGR) pulse sequence. Afterwards, multi-planar fast gradient echo
(MFGR) scans were performed with 8 various echo times (TEs) to
acquire images for R2* measurements. Regions of interest (ROIs) at
liver and muscle were measured using Advantage workstation.
Finally, the R2* was obtained by a linear regression of ln(sı) on TE.
The results showed that the longer the echo time, the smaller the signal
intensity. The R2* values of liver and muscle were 44.8 ± 10.9 s-1 and
37.4 ± 9.5 s-1, respectively. It implies that the iron concentration of
liver is higher than that of muscle. In conclusion, the more the iron
contents in tissue, the higher the R2*. The correlations between R2*
and iron content in NZW rabbits might be valuable for further
exploration.
Abstract: NiFe2O4 (nickel ferrite), ZnFe2O4 (zinc ferrite) and
Ni0.5Zn0.5Fe2O4 (nickel-zinc ferrite) were prepared by
mechanochemical route in a planetary ball mill starting from mixture
of the appropriate quantities of the Ni(OH)2/Fe(OH)3,
Zn(OH)2/Fe(OH)3 and Ni(OH)2/Zn(OH)2/Fe(OH)3 hydroxide
powders. In order to monitor the progress of chemical reaction and
confirm phase formation, powder samples obtained after 25 h, 18 h
and 10 h of milling were characterized by X-ray diffraction (XRD),
transmission electron microscopy (TEM), IR, Raman and Mössbauer
spectroscopy. It is shown that the soft mechanochemical method, i.e.
mechanochemical activation of hydroxides, produces high quality
single phase ferrite samples in much more efficient way. From the IR
spectroscopy of single phase samples it is obvious that energy of
modes depends on the ratio of cations. It is obvious that all samples
have more than 5 Raman active modes predicted by group theory in
the normal spinel structure. Deconvolution of measured spectra
allows one to conclude that all complex bands in the spectra are made
of individual peaks with the intensities that vary from spectrum to
spectrum. The deconvolution of Raman spectra allows to separate
contributions of different cations to a particular type of vibration and
to estimate the degree of inversion.
Abstract: Obturator Foramen is a specific structure in Pelvic
bone images and recognition of it is a new concept in medical image
processing. Moreover, segmentation of bone structures such as
Obturator Foramen plays an essential role for clinical research in
orthopedics. In this paper, we present a novel method to analyze the
similarity between the substructures of the imaged region and a hand
drawn template as a preprocessing step for computation of Pelvic
bone rotation on hip radiographs. This method consists of integrated
usage of Marker-controlled Watershed segmentation and Zernike
moment feature descriptor and it is used to detect Obturator Foramen
accurately. Marker-controlled Watershed segmentation is applied to
separate Obturator Foramen from the background effectively. Then,
Zernike moment feature descriptor is used to provide matching
between binary template image and the segmented binary image for
final extraction of Obturator Foramens. Finally, Pelvic bone rotation
rate calculation for each hip radiograph is performed automatically to
select and eliminate hip radiographs for further studies which depend
on Pelvic bone angle measurements. The proposed method is tested
on randomly selected 100 hip radiographs. The experimental results
demonstrated that the proposed method is able to segment Obturator
Foramen with 96% accuracy.
Abstract: Background: To compare the thinning patterns of the
ganglion cell-inner plexiform layer (GCIPL) and peripapillary retinal
nerve fiber layer (pRNFL) as measured using Cirrus high-definition
optical coherence tomography (HD-OCT) in patients with visual field
(VF) defects that respect the vertical meridian. Methods: Twenty eyes of eleven patients with VF defects that
respect the vertical meridian were enrolled retrospectively. The
thicknesses of the macular GCIPL and pRNFL were measured using
Cirrus HD-OCT. The 5% and 1% thinning area index (TAI) was
calculated as the proportion of abnormally thin sectors at the 5% and
1% probability level within the area corresponding to the affected VF.
The 5% and 1% TAI were compared between the GCIPL and pRNFL
measurements. Results: The color-coded GCIPL deviation map showed a
characteristic vertical thinning pattern of the GCIPL, which is also
seen in the VF of patients with brain lesions. The 5% and 1% TAI
were significantly higher in the GCIPL measurements than in the
pRNFL measurements (all P < 0.01). Conclusions: Macular GCIPL analysis clearly visualized a
characteristic topographic pattern of retinal ganglion cell (RGC) loss
in patients with VF defects that respect the vertical meridian, unlike
pRNFL measurements. Macular GCIPL measurements provide more
valuable information than pRNFL measurements for detecting the
loss of RGCs in patients with retrograde degeneration of the optic
nerve fibers.
Abstract: An experimental study with four different types of bed
conditions was carried out to understand the effect of roughness in
open channel flow at two different Reynolds numbers. The bed
conditions include a smooth surface and three different roughness
conditions, which were generated using sand grains with a median
diameter of 2.46 mm. The three rough conditions include a surface
with distributed roughness, a surface with continuously distributed
roughness and a sand bed with a permeable interface. A commercial
two-component fibre-optic LDA system was used to conduct the
velocity measurements. The variables of interest include the mean
velocity, turbulence intensity, correlation between the streamwise and
the wall normal turbulence, Reynolds shear stress and velocity triple
products. Quadrant decomposition was used to extract the magnitude
of the Reynolds shear stress of the turbulent bursting events. The
effect of roughness was evident throughout the flow depth. The
results show that distributed roughness has the greatest roughness
effect followed by the sand bed and the continuous roughness.
Compared to the smooth bed, the streamwise turbulence intensity
reduces but the vertical turbulence intensity increases at a location
very close to the bed due to the introduction of roughness. Although
the same sand grain is used to create the three different rough bed
conditions, the difference in the turbulence intensity is an indication
that the specific geometry of the roughness has an influence on
turbulence structure.
Abstract: The apportionment method is used by many countries, to calculate the distribution of seats in political bodies. For example, this method is used in the United States (U.S.) to distribute house seats proportionally based on the population of the electoral district. Famous apportionment methods include the divisor methods called the Adams Method, Dean Method, Hill Method, Jefferson Method and Webster Method. Sometimes the results from the implementation of these divisor methods are unfair and include errors. Therefore, it is important to examine the optimization of this method by using a bias measurement to figure out precise and fair results. In this research we investigate the bias of divisor methods in the U.S. Houses of Representatives toward large and small states by applying the Stolarsky Mean Method. We compare the bias of the apportionment method by using two famous bias measurements: the Balinski and Young measurement and the Ernst measurement. Both measurements have a formula for large and small states. The Third measurement however, which was created by the researchers, did not factor in the element of large and small states into the formula. All three measurements are compared and the results show that our measurement produces similar results to the other two famous measurements.
Abstract: Cole-Cole parameters of 40 post-menopausal women
are compared with their DEXA bone mineral density measurements.
Impedance characteristics of four extremities are compared; left and
right extremities are statistically same, but lower extremities are
statistically different than upper ones due to their different fat
content. The correlation of Cole-Cole impedance parameters to bone
mineral density (BMD) is observed to be higher for dominant arm.
With the post-menopausal population, ANOVA tests of the dominant
arm characteristic frequency, as a predictor for DEXA classified
osteopenic and osteoporic population around lumbar spine, is
statistically very significant. When used for total lumbar spine
osteoporosis diagnosis, the area under the Receiver Operating Curve
of the characteristic frequency is 0.830, suggesting that the Cole-Cole
plot characteristic frequency could be a useful diagnostic parameter
when integrated into standard screening methods for osteoporosis.
Moreover, the characteristic frequency can be directly measured by
monitoring frequency driven angular behavior of the dominant arm
without performing any complex calculation.
Abstract: This paper discusses the propagation of sound waves in
air, specifically in narrow rectangular pathways of an occluded-ear
simulator for acoustic measurements. In narrow pathways, both the
speed of sound and the phase of the sound waves are affected by the
damping of the air viscosity. Herein, we propose a new finite-element
method (FEM) that considers the effects of the air viscosity. The
method was developed as an extension of existing FEMs for porous,
sound-absorbing materials. The results of a numerical calculation for a
three-dimensional ear-simulator model using the proposed FEM were
validated by comparing with theoretical lumped-parameter modeling
analysis and standard values.
Abstract: The possibility of application the dietary fibers in
production of crackers was observed in this work, as well as their
influence on rheological and textural properties on the dough for
crackers and influence on sensory properties of obtained crackers.
Three different dietary fibers, oat, potato and pea fibers, replaced
10% of wheat flour. Long fermentation process and baking test
method were used for crackers production. The changes of dough for
crackers were observed by rheological methods of determination the
viscoelastic dough properties and by textural measurements. Sensory
quality of obtained crackers was described using quantity descriptive
method (QDA) by trained members of descriptive panel. Additional
analysis of crackers surface was performed by videometer. Based on
rheological determination, viscoelastic properties of dough for
crackers were reduced by application of dietary fibers. Manipulation
of dough with 10% of potato fiber was disabled, thus the recipe
modification included increase in water content at 35%. Dough
compliance to constant stress for samples with dietary fibers
decreased, due to more rigid and stiffer dough consistency compared
to control sample. Also, hardness of dough for these samples
increased and dough extensibility decreased. Sensory properties of
final products, crackers, were reduced compared to control sample.
Application of dietary fibers affected mostly hardness, structure and
crispness of the crackers. Observed crackers were low marked for
flavor and taste, due to influence of fibers specific aroma. The sample
with 10% of potato fibers and increased water content was the most
adaptable to applied stresses and to production process. Also this
sample was close to control sample without dietary fibers by
evaluation of sensory properties and by results of videometer method.
Abstract: In the field of fashion design, 3D Mannequin is a kind
of assisting tool which could rapidly realize the design concepts.
While the concept of 3D Mannequin is applied to the computer added
fashion design, it will connect with the development and the
application of design platform and system. Thus, the situation
mentioned above revealed a truth that it is very critical to develop a
module of 3D Mannequin which would correspond with the necessity
of fashion design. This research proposes a concrete plan that
developing and constructing a system of 3D Mannequin with Kinect.
In the content, ergonomic measurements of objective human features
could be attained real-time through the implement with depth camera
of Kinect, and then the mesh morphing can be implemented through
transformed the locations of the control-points on the model by
inputting those ergonomic data to get an exclusive 3D mannequin
model. In the proposed methodology, after the scanned points from the
Kinect are revised for accuracy and smoothening, a complete human
feature would be reconstructed by the ICP algorithm with the method
of image processing. Also, the objective human feature could be
recognized to analyze and get real measurements. Furthermore, the
data of ergonomic measurements could be applied to shape morphing
for the division of 3D Mannequin reconstructed by feature curves. Due
to a standardized and customer-oriented 3D Mannequin would be
generated by the implement of subdivision, the research could be
applied to the fashion design or the presentation and display of 3D
virtual clothes. In order to examine the practicality of research
structure, a system of 3D Mannequin would be constructed with JAVA
program in this study. Through the revision of experiments the
practicability-contained research result would come out.
Abstract: In the present study, response surface methodology has been used to optimize turn-assisted deep cold rolling process of AISI 4140 steel. A regression model is developed to predict surface hardness and surface roughness using response surface methodology and central composite design. In the development of predictive model, deep cold rolling force, ball diameter, initial roughness of the workpiece, and number of tool passes are considered as model variables. The rolling force and the ball diameter are the significant factors on the surface hardness and ball diameter and numbers of tool passes are found to be significant for surface roughness. The predicted surface hardness and surface roughness values and the subsequent verification experiments under the optimal operating conditions confirmed the validity of the predicted model. The absolute average error between the experimental and predicted values at the optimal combination of parameter settings for surface hardness and surface roughness is calculated as 0.16% and 1.58% respectively. Using the optimal processing parameters, the surface hardness is improved from 225 to 306 HV, which resulted in an increase in the near surface hardness by about 36% and the surface roughness is improved from 4.84µm to 0.252 µm, which resulted in decrease in the surface roughness by about 95%. The depth of compression is found to be more than 300µm from the microstructure analysis and this is in correlation with the results obtained from the microhardness measurements. Taylor hobson talysurf tester, micro vickers hardness tester, optical microscopy and X-ray diffractometer are used to characterize the modified surface layer.
Abstract: A model was constructed to predict the amount of
solar radiation that will make contact with the surface of the earth in
a given location an hour into the future. This project was supported
by the Southern Company to determine at what specific times during
a given day of the year solar panels could be relied upon to produce
energy in sufficient quantities. Due to their ability as universal
function approximators, an artificial neural network was used to
estimate the nonlinear pattern of solar radiation, which utilized
measurements of weather conditions collected at the Griffin, Georgia
weather station as inputs. A number of network configurations and
training strategies were utilized, though a multilayer perceptron with
a variety of hidden nodes trained with the resilient propagation
algorithm consistently yielded the most accurate predictions. In
addition, a modeled direct normal irradiance field and adjacent
weather station data were used to bolster prediction accuracy. In later
trials, the solar radiation field was preprocessed with a discrete
wavelet transform with the aim of removing noise from the
measurements. The current model provides predictions of solar
radiation with a mean square error of 0.0042, though ongoing efforts
are being made to further improve the model’s accuracy.
Abstract: Two finite element (FEM) models are presented in
this paper to address the random nature of the response of glued
timber structures made of wood segments with variable elastic
moduli evaluated from 3600 indentation measurements. This total
database served to create the same number of ensembles as was the
number of segments in the tested beam. Statistics of these ensembles
were then assigned to given segments of beams and the Latin
Hypercube Sampling (LHS) method was called to perform 100
simulations resulting into the ensemble of 100 deflections subjected
to statistical evaluation. Here, a detailed geometrical arrangement of
individual segments in the laminated beam was considered in the
construction of two-dimensional FEM model subjected to in fourpoint
bending to comply with the laboratory tests. Since laboratory
measurements of local elastic moduli may in general suffer from a
significant experimental error, it appears advantageous to exploit the
full scale measurements of timber beams, i.e. deflections, to improve
their prior distributions with the help of the Bayesian statistical
method. This, however, requires an efficient computational model
when simulating the laboratory tests numerically. To this end, a
simplified model based on Mindlin’s beam theory was established.
The improved posterior distributions show that the most significant
change of the Young’s modulus distribution takes place in laminae in
the most strained zones, i.e. in the top and bottom layers within the
beam center region. Posterior distributions of moduli of elasticity
were subsequently utilized in the 2D FEM model and compared with
the original simulations.
Abstract: The mixed micellization of adiphenine hydrochloride (ADP) with 1-decyl-3-methylimidazolium chloride (C10mim.Cl), was investigated at different mole fractions and temperatures by surface tension measurements. The synergistic behavior (i.e., non-ideal behavior) for binary mixtures was explained by the deviation of critical micelle concentration (cmc) from ideal critical micelle concentration (cmc*), micellar mole fraction (Xim) from ideal micellar mole fraction (Xiideal), the values of interaction parameter (β) and activity coefficients (fi) (for both mixed micelles and mixed monolayer). The excess free energy (ΔGex) for the ADP- C10mim.Cl binary mixtures explain the stability of mixed micelles in comparison to micelles of pure ADP and C10mim.Cl. Interfacial parameters, i.e., Gibbs surface excess (Гmax), minimum head group area at air/ water
interface (Amin), and free energy of micellization (ΔG0m) were also evaluated for the systems.
Abstract: The present work aims to throw light on the effects of
arcing in air on the surface state of contact pastilles made of silvernickel
Ag-Ni (60/40). Also, the photoelectric emission from these
electrical contacts has been investigated in the spectral range of 196-
256 nm. In order to study the effects of arcing on the EWF, the
metallic samples were subjected to electrical arcs in air, at
atmospheric pressure and room temperature, after that, they have
been introduced into the vacuum chamber of an experimental UHV
set-up for EWF measurements. Both Fowler method of isothermal
curves and linearized Fowler plots were used for the measurement of
the EWF by the photoelectric effect.
It has been found that the EWF varies with the number of applied
arcs. Thus, after 500 arcs in air, the observed EWF increasing is
probably due to progressive inclusion of oxide on alloy surface.
Microscopic examination is necessary to get better understandings on
EWF of silver alloys, for both virgin and arced electrical contacts.
Abstract: Monocopter is a single-wing rotary flying vehicle
which has the capability of hovering. This flying vehicle includes two
dynamic parts in which more efficiency can be expected rather than
other Micro UAVs due to the extended area of wing compared to its
fuselage. Low cost and simple mechanism in comparison to other
vehicles such as helicopter are the most important specifications of
this flying vehicle.
In the previous paper we discussed the introduction of the final
system but in this paper, the experimental design process of
Monocopter and its control algorithm has been investigated in
general. Also the editorial bugs in the previous article have been
corrected and some translational ambiguities have been resolved.
Initially by constructing several prototypes and carrying out many
flight tests the main design parameters of this air vehicle were
obtained by experimental measurements. Eventually the required
main monocopter for this project was constructed. After construction
of the monocopter in order to design, implementation and testing of
control algorithms first a simple optic system used for determining
the heading angle. After doing numerous tests on Test Stand, the
control algorithm designed and timing of applying control inputs
adjusted. Then other control parameters of system were tuned in
flight tests. Eventually the final control system designed and
implemented using the AHRS sensor and the final operational tests
performed successfully.
Abstract: Violet Sr–Al–O:Eu2+ phosphor particles were
synthesized from a metal–ethylenediaminetetraacetic acid (EDTA)
solution of Sr, Al, Eu, and particulate alumina via spray drying and
sintering in a reducing atmosphere. The crystal structures and emission
properties at 85–300 K were investigated. The composition of the
violet Sr–Al–O:Eu2+ phosphor particles was determined from various
Sr–Al–O:Eu2+ phosphors by their emission properties’ dependence
on temperature. The highly crystalline SrAl12O19:Eu2+ emission phases
were confirmed by their crystallite sizes and the activation energies for
the 4f5d–8S7/2 transition of the Eu2+ ion. These results showed that the
material identification for the violet Sr–Al–O:Eu2+ phosphor was
accomplished by the low-temperature luminescence measurements.
Abstract: This study is purposed to develop an efficient fault
detection method for Global Navigation Satellite Systems (GNSS)
applications based on adaptive noise covariance estimation. Due to the
dependence on radio frequency signals, GNSS measurements are
dominated by systematic errors in receiver’s operating environment.
In the proposed method, the pseudorange and carrier-phase
measurement noise covariances are obtained at time propagations and
measurement updates in process of Carrier-Smoothed Code (CSC)
filtering, respectively. The test statistics for fault detection are
generated by the estimated measurement noise covariances. To
evaluate the fault detection capability, intentional faults were added to
the filed-collected measurements. The experiment result shows that
the proposed method is efficient in detecting unhealthy measurements
and improves GNSS positioning accuracy against fault occurrences.
Abstract: This article presents summary on preparation and
characterization of zinc, copper, cadmium and cobalt chromite
nanocrystals, embedded in an amorphous silica matrix. The
ZnCr2O4/SiO2, CuCr2O4/SiO2, CdCr2O4/SiO2 and CoCr2O4/SiO2
nanocomposites were prepared by a conventional sol-gel method
under acid catalysis. Final heat treatment of the samples was carried
out at temperatures in the range of 900−1200 ◦C to adjust the
phase composition and the crystallite size, respectively. The resulting
samples were characterized by Powder X-ray diffraction (PXRD),
High Resolution Transmission Electron Microscopy (HRTEM),
Raman/FTIR spectroscopy and magnetic measurements. Formation
of the spinel phase was confirmed in all samples. The average size of
the nanocrystals was determined from the PXRD data and by direct
particle size observation on HRTEM; both results were correlated.
The mean particle size (reviewed by HRTEM) was in the range from
∼4 to 46 nm. The results showed that the sol-gel method can be
effectively used for preparation of the spinel chromite nanoparticles
embedded in the silica matrix and the particle size is driven by the
type of the cation A2+ in the spinel structure and the temperature
of the final heat treatment. Magnetic properties of the nanocrystals
were found to be just moderately modified in comparison to the bulk
phases.