Abstract: This paper presents a simple and sensitive kinetic
spectrophotometric method for the determination of ramipril in
commercial dosage forms. The method is based on the reaction of the
drug with 1-chloro-2,4-dinitrobenzene (CDNB) in dimethylsulfoxide
(DMSO) at 100 ± 1ºC. The reaction is followed
spectrophotometrically by measuring the rate of change of the
absorbance at 420 nm. Fixed-time (ΔA) and equilibrium methods are
adopted for constructing the calibration curves. Both the calibration
curves were found to be linear over the concentration ranges 20 - 220
μg/ml. The regression analysis of calibration data yielded the linear
equations: Δ A = 6.30 × 10-4 + 1.54 × 10-3 C and A = 3.62 × 10-4 +
6.35 × 10-3 C for fixed time (Δ A) and equilibrium methods,
respectively. The limits of detection (LOD) for fixed time and
equilibrium methods are 1.47 and 1.05 μg/ml, respectively. The
method has been successfully applied to the determination of ramipril
in commercial dosage forms. Statistical comparison of the results
shows that there is no significant difference between the proposed
methods and Abdellatef-s spectrophotometric method.
Abstract: In this paper we present a general formalism for the
establishment of the family of selective regressor affine projection
algorithms (SR-APA). The SR-APA, the SR regularized APA (SR-RAPA),
the SR partial rank algorithm (SR-PRA), the SR binormalized
data reusing least mean squares (SR-BNDR-LMS), and the SR normalized
LMS with orthogonal correction factors (SR-NLMS-OCF)
algorithms are established by this general formalism. We demonstrate
the performance of the presented algorithms through simulations in
acoustic echo cancellation scenario.
Abstract: Deoxygenation of beef fat for the production of hydrogenated biodiesel is investigated in a high pressure continuous flow fixed bed reactor over palladium-supported mesoporous titania catalyst synthesized via a combined single-step sol-gel process with surfactant-assisted templating method (SATM). The catalyst possessed a mesoporous charactheristic with high surface area and narrow pore size distribution. The main products of all Pd/TiO2 catalysts are n-heptadecane (n-C17) and n-pentadecane (n-C15) resulting from decarbonylation reaction. Pd/TiO2 catalyst synthesized via a combined single-step sol-gel process with SATM (SSSG) gave higher activity and selectivity to the desired products when compared to IWI/SG-TiO2 and IWI/P25-TiO2, respectively. SSSG catalyst gave the average conversion up to 80-90 % and 80 % for the selectivity in diesel range hydrocarbons. This result may cause by the higher surface area and the ability in dispersion of palladium ion in mesoporous of TiO2 during sol-gel process.
Abstract: Testing accounts for the major percentage of technical
contribution in the software development process. Typically, it
consumes more than 50 percent of the total cost of developing a
piece of software. The selection of software tests is a very important
activity within this process to ensure the software reliability
requirements are met. Generally tests are run to achieve maximum
coverage of the software code and very little attention is given to the
achieved reliability of the software. Using an existing methodology,
this paper describes how to use Bayesian Belief Networks (BBNs) to
select unit tests based on their contribution to the reliability of the
module under consideration. In particular the work examines how the
approach can enhance test-first development by assessing the quality
of test suites resulting from this development methodology and
providing insight into additional tests that can significantly reduce
the achieved reliability. In this way the method can produce an
optimal selection of inputs and the order in which the tests are
executed to maximize the software reliability. To illustrate this
approach, a belief network is constructed for a modern software
system incorporating the expert opinion, expressed through
probabilities of the relative quality of the elements of the software,
and the potential effectiveness of the software tests. The steps
involved in constructing the Bayesian Network are explained as is a
method to allow for the test suite resulting from test-driven
development.
Abstract: Multi-site damage (MSD) has been a challenge to
aircraft, civil and power plant structures. In real life components are subjected to cracking at many vulnerable locations such as the bolt
holes. However, we do not consider for the presence of multiple cracks. Unlike components with a single crack, these components are
difficult to predict. When two cracks approach one another, their
stress fields influence each other and produce enhancing or shielding effect depending on the position of the cracks. In the present study,
numerical studies on fracture analysis have been conducted by using
the developed code based on the modified virtual crack closure integral (MVCCI) technique and finite element analysis (FEA) software ABAQUS for computing SIF of plates with multiple cracks.
Various parametric studies have been carried out and the results have
been compared with literature where ever available and also with the solution, obtained by using ABAQUS. By conducting extensive
numerical studies expressions for SIF have been obtained for collinear cracks and non-aligned cracks.
Abstract: A glider is in essence an unpowered vehicle and in this project we designed and built an oceanic glider, designed to operate underwater. This Glider was designed to collect ocean data such as temperature, pressure and (in future measures physical dimensions of the operating environment) and output this data to an external source. Development of the Oceanic Glider required research into various actuation systems that control buoyancy, pitch and yaw and the dynamics of these systems. It also involved the design and manufacture of the Glider and the design and implementation of a controller that enabled the Glider to navigate and move in an appropriate manner.
Abstract: Environmental statistics reveals that the pollution of
acid rain in South Korea is a serious issue. Yet the awareness of people
is low. Even after a gradual decrease of pollutant emission in Korea,
the acidity has not been reduced. There no boundaries in the
atmosphere are set and the influence of the neighboring countries such
as China is apparent. Governmental efforts among China, Japan and
Korea have been made on this issue. However, not much progress has
been observed. Along with the governmental activities, therefore, an
active monitoring of the pollution among the countries and the
promotion of environmental awareness at the civil level including
especially the middle and high schools are highly recommended. It
will be this young generation who will face damaged country as
inheritance not the current generation.
Abstract: The pavement constructions on soft and expansive soils are not durable and unable to sustain heavy traffic loading. As a result, pavement failures and settlement problems will occur very often even under light traffic loading due to cyclic and rolling effects. Geotechnical engineers have dwelled deeply into this matter, and adopt various methods to improve the engineering characteristics of soft fine-grained soils and expansive soils. The problematic soils are either replaced by good and better quality material or treated by using chemical stabilization with various binding materials. Increased the strength and durability are also the part of the sustainability drive to reduce the environment footprint of the built environment by the efficient use of resources and waste recycle materials. This paper presents a series of laboratory tests and evaluates the effect of cement and fly ash on the strength and drainage characteristics of soil in Miri. The tests were performed at different percentages of cement and fly ash by dry weight of soil. Additional tests were also performed on soils treated with the combinations of fly ash with cement and lime. The results of this study indicate an increase in unconfined compression strength and a decrease in hydraulic conductivity of the treated soil.
Abstract: In this paper, we propose a novel time-frequency distribution (TFD) for the analysis of multi-component signals. In particular, we use synthetic as well as real-life speech signals to prove the superiority of the proposed TFD in comparison to some existing ones. In the comparison, we consider the cross-terms suppression and the high energy concentration of the signal around its instantaneous frequency (IF).
Abstract: A piston cylinder based high pressure differential
thermal analyzer system is developed to investigate phase
transformations, melting, glass transitions, crystallization behavior of
inorganic materials, glassy systems etc., at ambient to 4 GPa and at
room temperature to 1073 K. The pressure is calibrated by the phase
transition of bismuth and ytterbium and temperature is calibrated
by using thermocouple data chart. The system developed is
calibrated using benzoic acid, ammonium nitrate and it has a
pressure and temperature control of ± 8.9 x 10 -4 GPa , ± 2 K
respectively. The phase transition of Asx Te100-x chalcogenides,
ferrous oxide and strontium boride are studied using the
indigenously developed system.
Abstract: Cerium-doped lanthanum bromide LaBr3:Ce(5%)
crystals are considered to be one of the most advanced scintillator
materials used in PET scanning, combining a high light yield, fast
decay time and excellent energy resolution. Apart from the correct
choice of scintillator, it is also important to optimise the detector
geometry, not least in terms of source-to-detector distance in order to
obtain reliable measurements and efficiency. In this study a
commercially available 25 mm x 25 mm BrilLanCeTM 380 LaBr3: Ce
(5%) detector was characterised in terms of its efficiency at varying
source-to-detector distances. Gamma-ray spectra of 22Na, 60Co, and
137Cs were separately acquired at distances of 5, 10, 15, and 20cm. As
a result of the change in solid angle subtended by the detector, the
geometric efficiency reduced in efficiency with increasing distance.
High efficiencies at low distances can cause pulse pile-up when
subsequent photons are detected before previously detected events
have decayed. To reduce this systematic error the source-to-detector
distance should be balanced between efficiency and pulse pile-up
suppression as otherwise pile-up corrections would need to be
necessary at short distances. In addition to the experimental
measurements Monte Carlo simulations have been carried out for the
same setup, allowing a comparison of results. The advantages and
disadvantages of each approach have been highlighted.
Abstract: The use of bioindicators plants (lichens, bryophytes
and Sphagnum....) in monitoring pollution by heavy metals has been
the subject of several works. However, few studies have addressed
the impact of specific type-s pollutants (fertilizers, pesticides.) on
these organisms.
We propose in this work to make the highlighting effect of NPKs
(NPK: nitrogen-phosphate-potassium-sulfate (NP2O5K2O) (15,15,15),
at concentrations of 10, 20, 30 , 40 and 50mM/L) on the activity of
detoxification enzymes (GSH/GST, CAT, APX and MDA) of plant
bioindicators (mosses and lichens) after treatment for 3 and 7 days.
This study shows the important role of the defense system in the
accumulation and tolerance to chemical pollutants through the
activation of enzymatic (GST (glutathione-S-transferase, APX
(ascorbat peroxidase), CAT (catalase)) and nonenzymatic biomarkers
(GSH (glutathione), MDA (malondialdehyde)) against oxidative
stress generated by the NPKs.
Abstract: Recently, lots of researchers are attracted to retrieving
multimedia database by using some impression words and their values.
Ikezoe-s research is one of the representatives and uses eight pairs of
opposite impression words. We had modified its retrieval interface and
proposed '2D-RIB'. In '2D-RIB', after a retrieval person selects a
single basic music, the system visually shows some other music
around the basic one along relative position. He/she can select one of
them fitting to his/her intention, as a retrieval result. The purpose of
this paper is to improve his/her satisfaction level to the retrieval result
in 2D-RIB. One of our extensions is to define and introduce the
following two measures: 'melody goodness' and 'general acceptance'.
We implement them in different five combinations. According to an
evaluation experiment, both of these two measures can contribute to
the improvement. Another extension is three types of customization.
We have implemented them and clarified which customization is
effective.
Abstract: The primary cause of Total Hip Replacement (THR)
failure for younger patients is aseptic loosening. This complication is
twice more likely to happen in acetabular cup than in femoral stem.
Excessive micromotion between bone and implant will cause
loosening and it depends in patient activities, age and bone. In this
project, the effects of different metal back design of press fit on
osseointegration of the acetabular cup are carried out. Commercial
acetabular cup designs, namely Spiked, Superfix and Quadrafix are
modelled and analyzed using commercial finite element software.
The diameter of acetabular cup is based on the diameter of acetabular
rim to make sure the component fit to the acetabular cavity. A new
design of acetabular cup are proposed and analyzed to get better
osseointegration between the bones and implant interface. Results
shows that the proposed acetabular cup designs are more stable
compared to other designs with respect to stress and displacement
aspects.
Abstract: The purpose of this study was to explore the complex
flow structure a novel active-type micromixer that based on concept of
Wankle-type rotor. The characteristics of this micromixer are two
folds; a rapid mixing of reagents in a limited space due to the
generation of multiple vortices and a graduate increment in dynamic
pressure as the mixed reagents is delivered to the output ports.
Present micro-mixer is consisted of a rotor with shape of triangle
column, a blending chamber and several inlet and outlet ports. The
geometry of blending chamber is designed to make the rotor can be
freely internal rotated with a constant eccentricity ratio. When the
shape of the blending chamber and the rotor are fixed, the effects of
rotating speed of rotor and the relative locations of ports on the mixing
efficiency are numerical studied. The governing equations are
unsteady, two-dimensional incompressible Navier-Stokes equation
and the working fluid is the water. The species concentration equation
is also solved to reveal the mass transfer process of reagents in various
regions then to evaluate the mixing efficiency.
The dynamic mesh technique was implemented to model the
dynamic volume shrinkage and expansion of three individual
sub-regions of blending chamber when the rotor conducted a complete
rotating cycle. Six types of ports configuration on the mixing
efficiency are considered in a range of Reynolds number from 10 to
300. The rapid mixing process was accomplished with the multiple
vortex structures within a tiny space due to the equilibrium of shear
force, viscous force and inertial force. Results showed that the highest
mixing efficiency could be attained in the following conditions: two
inlet and two outlet ports configuration, that is an included angle of 60
degrees between two inlets and an included angle of 120 degrees
between inlet and outlet ports when Re=10.
Abstract: Images of human iris contain specular highlights due
to the reflective properties of the cornea. This corneal reflection
causes many errors not only in iris and pupil center estimation but
also to locate iris and pupil boundaries especially for methods that
use active contour. Each iris recognition system has four steps:
Segmentation, Normalization, Encoding and Matching. In order to
address the corneal reflection, a novel reflection removal method is
proposed in this paper. Comparative experiments of two existing
methods for reflection removal method are evaluated on CASIA iris
image databases V3. The experimental results reveal that the
proposed algorithm provides higher performance in reflection
removal.
Abstract: The aim of current study was to investigate the
changes in the quality parameters of Holstein bull semen during the
heat stress and the effect of feeding a source of omega-3 fatty acids
in this period. Samples were obtained from 19 Holstein bulls during
the expected time of heat stress in Iran (June to September 2009).
Control group (n=10) were fed a standard concentrate feed while
treatment group (n=9) had this feed top dressed with 100 g of an
omega-3 enriched nutriceutical. Semen quality was assessed on
ejaculates collected after 1, 5, 9 and 12 weeks of supplementation.
Computer-assisted assessment of sperm motility, viability (eosinnigrosin)
and hypo-osmotic swelling test (HOST) were conducted.
Heat stress affected sperm quality parameters by week 5 and 9
(p
Abstract: This paper proposes the concept of aerocapture with
aerodynamic-environment-adaptive variable geometry flexible
aeroshell that vehicle deploys. The flexible membrane is composed
of thin-layer film or textile as its aeroshell in order to solve some
problems obstructing realization of aerocapture technique.
Multi-objective optimization study is conducted to investigate
solutions and derive design guidelines. As a result, solutions which
can avoid aerodynamic heating and enlarge the corridor width up
to 10% are obtained successfully, so that the effectiveness of this
concept can be demonstrated. The deformation-use optimum
solution changes its drag coefficient from 1.6 to 1.1, along with the
change in dynamic pressure. Moreover, optimization results show
that deformation-use solution requires the membrane for which
upper temperature limit and strain limit are more than 700 K and
120%, respectively, and elasticity (Young-s modulus) is of order of
106 Pa.
Abstract: A free-trade agreement is found to increase Thailand-s
agricultural imports from New Zealand, despite the short span of
time for which the agreement has been operational. The finding is
described by autoregressive estimates that correct for possible unit
roots in the data. The agreement-s effect upon imports is also
estimated while considering an error-correction model of imports
against gross domestic product.
Abstract: The past decade has witnessed a good opportunities
for city development schemes in UK. The government encouraged
restoration of city centers to comprise mixed use developments with
high density residential apartments. Investments in regeneration areas
were doing well according to the analyses of Property Databank
(IPD). However, more recent analysis by IPD has shown that since
2007, property in regeneration areas has been more vulnerable to the
market downturn than other types of investment property. The early
stages of a property market downturn may be felt most in
regeneration where funding, investor confidence and occupier
demand would dissipate because the sector was considered more
marginal or risky when development costs rise. Moreover, the Bank
of England survey shows that lenders have sequentially tightened the
availability of credit for commercial real estate since mid-2007. A
sharp reduction in the willingness of banks to lend on commercial
property was recorded. The credit crunch has already affected
commercial property but its impact has been particularly severe in
certain kinds of properties where residential developments are
extremely difficult, in particular city centre apartments and buy-to-let
markets. Commercial property – retail, industrial leisure and mixed
use were also pressed, in Birmingham; tens of mixed use plots were
built to replace old factories in the heart of the city. The purpose of
these developments was to enable young professionals to work and
live in same place. Thousands of people lost their jobs during the
recession, moreover lending was more difficult and the future of
many developments is unknown. The recession casts its shadow upon
the society due to cuts in public spending by government, Inflation,
rising tuition fees and high rise in unemployment generated anger and
hatred was spreading among youth causing vandalism and riots in
many cities. Recent riots targeted many mixed used development in
the UK where banks, shops, restaurants and big stores were robbed
and set into fire leaving residents with horror and shock. This paper
examines the impact of the recession and riots on mixed use
development in UK.