Abstract: The aim of this study is to present the results of a retrospective survey on the foreign matter found in foods analyzed at the Adolfo Lutz Institute, from July 2001 to July 2015. All the analyses were conducted according to the official methods described on Association of Official Agricultural Chemists (AOAC) for the micro analytical procedures and Food and Drug Administration (FDA) for the macro analytical procedures. The results showed flours, cereals and derivatives such as baking and pasta products were the types of food where foreign matters were found more frequently followed by condiments and teas. Fragments of stored grains insects, its larvae, nets, excrement, dead mites and rodent excrement were the most foreign matter found in food. Besides, foreign matters that can cause a physical risk to the consumer’s health such as metal, stones, glass, wood were found but rarely. Miscellaneous (shell, sand, dirt and seeds) were also reported. There are a lot of extraneous materials that are considered unavoidable since are something inherent to the product itself, such as insect fragments in grains. In contrast, there are avoidable extraneous materials that are less tolerated because it is preventable with the Good Manufacturing Practice. The conclusion of this work is that although most extraneous materials found in food are considered unavoidable it is necessary to keep the Good Manufacturing Practice throughout the food processing as well as maintaining a constant surveillance of the production process in order to avoid accidents that may lead to occurrence of these extraneous materials in food.
Abstract: The great majority of the applications of thermal isolation in the strip of drops and averages temperatures (up to 200ºC), it is made of materials aggressive nature, such an as glass wool, rock wool, polystyrene, EPS among others. Such materials, in spite of the effectiveness in the retention of the flow of heat, possess considerable cost and when discarded they are long years to be to decompose. In that context, trying to adapt the world politics the about of the preservation of the environment, a study began with intention of developing a material composite, with properties of thermal, originating from insulating industrial residues. In this research, the behavior of the composite was analyzed, as submitted the fire. For this, the reaction rehearsals were accomplished to the fire for the composites 2:1; 1:1; 1:2 and for the Latex, based in the "con" experiment in agreement with the norm ASTM - E 1334 - 90. As consequence, in function of the answers of the system was possible to be observed to the acting of each mixture proportion.
Abstract: In this paper, shear behavior of reconstituted clay reinforced with varying diameter of sand compaction piles with area replacement-ratio (as) of 6.25, 10.24, 16, 20.25 and 64% in 100mm diameter and 200mm long clay specimens is modeled using consolidated drained and undrained triaxial tests under different confining pressures ranging from 50kPa to 575kPa. The test results show that the stress-strain behavior of the clay was highly influenced by the presence of SCP. The insertion of SCPs into soft clay has shown to have a positive effect on the load carrying capacity of the clay, resulting in a composite soil mass that has greater shear strength and improved stiffness compared to the unreinforced clay due to increased reinforcement area ratio. In addition, SCP also acts as vertical drain in the clay thus accelerating the dissipation of excess pore water pressures that are generated during loading by shortening the drainage path and activating radial drainage, thereby reducing post-construction settlement. Thus, sand compaction piles currently stand as one of the most viable and practical techniques for improving the mechanical properties of soft clays.
Abstract: The objective of this study was to synthesize and characterize 5-acryloyloxy-3,4-dichlorocrotonolactone (a furanone derivative), use this derivative to modify a dental restorative, and study the effect of the derivative on the antibacterial activity and compressive strength of the formed restorative. In this study, a furanone derivative was synthesized, characterized, and used to formulate a dental restorative. Compressive strength (CS) and S. mutans viability were used to evaluate the mechanical strength and antibacterial activity of the formed restorative. The fabricated restorative specimens were photocured and conditioned in distilled water at 37oC for 24 h, followed by direct testing for CS or/and incubating with S. mutans for 48 h for antibacterial testing. The results show that the modified dental restorative showed a significant antibacterial activity without substantially decreasing the mechanical strengths. With addition of the antibacterial derivative up to 30%, the restorative kept its original CS nearly unchanged but showed a significant antibacterial activity with 68% reduction in the S. mutans viability. Furthermore, the antibacterial function of the modified restorative was not affected by human saliva. The aging study also indicates that the modified restorative may have a long-lasting antibacterial function. It is concluded that this experimental antibacterial restorative may potentially be developed into a clinically attractive dental filling restorative due to its high mechanical strength and antibacterial function.
Abstract: In many practical situations, bubbles are dispersed in a
liquid phase. Understanding these complex bubbly flows is therefore
a key issue for applications such as shell and tube heat exchangers,
mineral flotation and oxidation in water treatment. Although a large
body of work exists for bubbles rising in an unbounded medium,
that of bubbles rising in constricted geometries has received less
attention. The particular case of a bubble sliding underneath an
inclined surface is common to two-phase flow systems. The current
study intends to expand this knowledge by performing experiments
to quantify the streamwise flow structures associated with a single
sliding air bubble under an inclined surface in quiescent water. This
is achieved by means of two-dimensional, two-component particle
image velocimetry (PIV), performed with a continuous wave laser
and high-speed camera. PIV vorticity fields obtained in a plane
perpendicular to the sliding surface show that there is significant bulk
fluid motion away from the surface. The associated momentum of the
bubble means that this wake motion persists for a significant time
before viscous dissipation. The magnitude and direction of the flow
structures in the streamwise measurement plane are found to depend
on the point on its path through which the bubble enters the plane.
This entry point, represented by a phase angle, affects the nature and
strength of the vortical structures. This study reconstructs the vorticity
field in the wake of the bubble, converting the field at different
instances in time to slices of a large-scale wake structure. This is, in
essence, Taylor’s ”frozen turbulence” hypothesis. Applying this to the
vorticity fields provides a pseudo three-dimensional representation
from 2-D data, allowing for a more intuitive understanding of the
bubble wake. This study provides insights into the complex dynamics
of a situation common to many engineering applications, particularly
shell and tube heat exchangers in the nucleate boiling regime.
Abstract: Promotion of the Fiber Reinforced Concrete (FRC) as a construction material for civil engineering projects has invoked numerous researchers to investigate their mechanical behavior. Even though there is satisfactory information about the effects of fiber type and length, concrete mixture, casting type and other variables on the strength and deformability parameters of FRC, the numerical modeling of such materials still needs research attention. The focus of this study is to investigate the feasibility of Concrete Damaged Plasticity (CDP) model in prediction of Macro-synthetic FRC structures behavior. CDP model requires the tensile behavior of concrete to be well characterized. For this purpose, a series of uniaxial direct tension and four point bending tests were conducted on the notched specimens to define bilinear tension softening (post-peak tension stress-strain) behavior. With these parameters obtained, the flexural behavior of macro-synthetic FRC beams were modeled and the results showed a good agreement with the experimental measurements.
Abstract: Reinforced concrete (RC) shear wall system of residential buildings is popular in South Korea. RC walls are subjected to axial forces in common and the effect of axial forces on the strength loss of the fire damaged walls has not been investigated. This paper aims at investigating temperature distribution on fire damaged concrete walls having different axial loads. In the experiments, a variable of specimens is axial force ratio. RC walls are fabricated with 150mm of wall thicknesses, 750mm of lengths and 1,300mm of heights having concrete strength of 24MPa. After curing, specimens are heated on one surface with ISO-834 standard time-temperature curve for 2 hours and temperature distributions during the test are measured using thermocouples inside the walls. The experimental results show that the temperature of the RC walls exposed to fire increases as axial force ratio increases. To verify the experiments, finite element (FE) models are generated for coupled temperature-structure analyses. The analytical results of thermal behaviors are in good agreement with the experimental results. The predicted displacement of the walls decreases when the axial force increases.
Abstract: This work studies the effect of thickness on structural
and electrical properties of CuAlS2 thin films grown by two stage
vacuum thermal evaporation technique. CuAlS2 thin films of
thicknesses 50nm, 100nm and 200nm were deposited on suitably
cleaned corning 7059 glass substrate at room temperature (RT). In
the first stage Cu-Al precursors were grown at room temperature by
thermal evaporation and in the second stage Cu-Al precursors were
converted to CuAlS2 thin films by sulfurisation under sulfur
atmosphere at the temperature of 673K. The structural properties of
the films were examined by X-ray diffraction (XRD) technique while
electrical properties of the specimens were studied using four point
probe method. The XRD studies revealed that the films are of
crystalline in nature having tetragonal structure. The variations of the
micro-structural parameters, such as crystallite size (D), dislocation
density ( ), and micro-strain ( ), with film thickness were
investigated. The results showed that the crystallite sizes increase as
the thickness of the film increases. The dislocation density and
micro-strain decreases as the thickness increases. The resistivity ( )
of CuAlS2 film is found to decrease with increase in film thickness,
which is related to the increase of carrier concentration with film
thickness. Thus thicker films exhibit the lowest resistivity and high
carrier concentration, implying these are the most conductive films.
Low electrical resistivity and high carrier concentration are widely
used as the essential components in various optoelectronic devices
such as light-emitting diode and photovoltaic cells.
Abstract: The effect of upstream surface roughness over a
smooth forward facing step in an open channel was investigated
using a particle image velocimetry technique. Three different
upstream surface topographies consisting of hydraulically smooth
wall, sandpaper 36 grit and sand grains were examined. Besides the
wall roughness conditions, all other upstream flow characteristics
were kept constant. It was also observed that upstream roughness
decreased the approach velocity by 2% and 10% but increased the
turbulence intensity by 14% and 35% at the wall-normal distance
corresponding to the top plane of the step compared to smooth
upstream. The results showed that roughness decreased the
reattachment lengths by 14% and 30% compared to smooth upstream.
Although the magnitudes of maximum positive and negative
Reynolds shear stress in separated and reattached region were 0.02Ue
for all the cases, the physical size of both the maximum and
minimum contour levels were decreased by increasing upstream
roughness.
Abstract: The tribological test with Pin-On-Disc configuration
measures friction and wear properties in dry or lubricated sliding
surfaces of a variety of materials and coatings. Polymeric matrix
composites loaded with mineral filler were used, 1%, 3%, 10%, 30%,
and 50% mass percentage of filler, to reduce the material cost by
using mineral tailings. Using a pin-on-disc tribometer to quantify
coefficient of friction and wear resistance of the specimens. The
parameters known to performing the test were 300 rpm rotation,
normal load of 16N and duration of 33.5 minutes. The composite
with 10% mineral filler performed better, considering that the wear
resistance was good when compared to the other compositions and an
average low coefficient of friction, in the order of μ ≤ 0.15.
Abstract: The combination of the properties of graphene oxide
(OG) and PVDF homopolymer makes their combined composite
materials as multifunctional systems with great potential. Knowledge
of the molecular structure is essential for better use. In this work, the
degradation of PVDF polymer exposed to gamma irradiation in
oxygen atmosphere in high dose rate has been studied and compared
to degradation of PVDF/OG composites. The samples were irradiated
with a Co-60 source at constant dose rate, with doses ranging from
100 kGy to 1,000 kGy. In FTIR data shown that the formation of
oxidation products was at the both samples with formation of
carbonyl and hydroxyl groups amongst the most prevalent products
in the pure PVDF samples. In the other hand, the composites samples
exhibit less presence of degradation products with predominant
formation of carbonyl groups, these results also seen in the UV-Vis
analysis. The results show that the samples of composites may have
greater resistance to the irradiation process, since they have less
degradation products than pure PVDF samples seen by spectroscopic
techniques.
Abstract: The exploitation of flow pulsation in micro- and
mini-channels is a potentially useful technique for enhancing cooling
of high-end photonics and electronics systems. It is thought that
pulsation alters the thickness of the hydrodynamic and thermal
boundary layers, and hence affects the overall thermal resistance
of the heat sink. Although the fluid mechanics and heat transfer
are inextricably linked, it can be useful to decouple the parameters
to better understand the mechanisms underlying any heat transfer
enhancement. Using two-dimensional, two-component particle image
velocimetry, the current work intends to characterize the heat transfer
mechanisms in pulsating flow with a mean Reynolds number of
48 by experimentally quantifying the hydrodynamics of a generic
liquid-cooled channel geometry. Flows circulated through the test
section by a gear pump are modulated using a controller to achieve
sinusoidal flow pulsations with Womersley numbers of 7.45 and
2.36 and an amplitude ratio of 0.75. It is found that the transient
characteristics of the measured velocity profiles are dependent on the
speed of oscillation, in accordance with the analytical solution for
flow in a rectangular channel. A large velocity overshoot is observed
close to the wall at high frequencies, resulting from the interaction
of near-wall viscous stresses and inertial effects of the main fluid
body. The steep velocity gradients at the wall are indicative of
augmented heat transfer, although the local flow reversal may reduce
the upstream temperature difference in heat transfer applications.
While unsteady effects remain evident at the lower frequency, the
annular effect subsides and retreats from the wall. The shear rate at
the wall is increased during the accelerating half-cycle and decreased
during deceleration compared to steady flow, suggesting that the flow
may experience both enhanced and diminished heat transfer during
a single period. Hence, the thickness of the hydrodynamic boundary
layer is reduced for positively moving flow during one half of the
pulsation cycle at the investigated frequencies. It is expected that the
size of the thermal boundary layer is similarly reduced during the
cycle, leading to intervals of heat transfer enhancement.
Abstract: In this study, thermal fatigue properties of 400 series
ferritic stainless steels have been evaluated in the temperature ranges
of 200-800oC and 200-900oC. Systematic methods for control of
temperatures within the predetermined range and measurement of load
applied to specimens as a function of temperature during thermal
cycles have been established. Thermal fatigue tests were conducted
under fully constrained condition, where both ends of specimens were
completely fixed. It has been revealed that load relaxation behavior at
the temperatures of thermal cycle was closely related with the thermal
fatigue property. Thermal fatigue resistance of 430J1L stainless steel
is found to be superior to the other steels.
Abstract: Asphalt pavement itself is a mixture made up of mainly aggregates, binders, and fillers that acts as a composition used for pavement construction. An experimental program was setup to determine the fatigue performance test of Asphalt with three different grades of conventional binders. Asphalt specimen has achieved the maximum optimum bulk density and air voids with a consistent bulk density of 2.3 t/m3, with an air void of 5% ± 0.5, before loading into the Asphalt Mixture Performance Tested (AMPT) for fatigue test. The number of cycles is defined as the point where phase angle drops, which is caused by the formation of cracks due to the increasing micro cracks when asphalt is undergoing repeated cycles of loading. Thus, the data collected are analyzed using the drop of phase angle as failure criteria. Based in the data analyzed, it is evident that the fatigue life of asphalt lies on the grade of binder. The result obtained shows that all specimens do experience a drop in phase angle due to macro cracks in the asphalt specimen.
Abstract: Microstructure and mechanical properties of AZ91D
Mg alloys for nonflammable use, containing Ca and Y, were
investigated in this study. Solid solution treatment of AZ91D Mg alloy
with Ca and Y was successfully conducted at 420oC and
supersaturated microstructure with almost all beta phases resolved into
matrix was obtained. After solid solution treatment, the alloy was
annealed at temperatures of 180 and 200oC for time intervals from 1
min to 48 hrs and hardness of each condition was measured by
micro-Vickers method. Peak aging conditions were deduced from the
results as at the temperature of 200oC for 10 hrs. Hot rolling was also
carried out at 400oC by the reduction ratio of 0.6 through 5 passes
followed by recrystallization treatment. Tensile and compressive
properties were measured at room temperature on the specimens of
each process, i.e. as-cast, solution treatment, hot rolling, and
recrystallization.
Abstract: This paper outlines the development of an
experimental technique in quantifying supersonic jet flows, in an
attempt to avoid seeding particle problems frequently associated with
particle-image velocimetry (PIV) techniques at high Mach numbers.
Based on optical flow algorithms, the idea behind the technique
involves using high speed cameras to capture Schlieren images of the
supersonic jet shear layers, before they are subjected to an adapted
optical flow algorithm based on the Horn-Schnuck method to
determine the associated flow fields. The proposed method is capable
of offering full-field unsteady flow information with potentially
higher accuracy and resolution than existing point-measurements or
PIV techniques. Preliminary study via numerical simulations of a
circular de Laval jet nozzle successfully reveals flow and shock
structures typically associated with supersonic jet flows, which serve
as useful data for subsequent validation of the optical flow based
experimental results. For experimental technique, a Z-type Schlieren
setup is proposed with supersonic jet operated in cold mode,
stagnation pressure of 4 bar and exit Mach of 1.5. High-speed singleframe
or double-frame cameras are used to capture successive
Schlieren images. As implementation of optical flow technique to
supersonic flows remains rare, the current focus revolves around
methodology validation through synthetic images. The results of
validation test offers valuable insight into how the optical flow
algorithm can be further improved to improve robustness and
accuracy. Despite these challenges however, this supersonic flow
measurement technique may potentially offer a simpler way to
identify and quantify the fine spatial structures within the shock shear
layer.
Abstract: The paper presents an additive manufacturing process for the production of metal and composite parts. It is termed as composite metal foil manufacturing and is a combination of laminated object manufacturing and brazing techniques. The process has been described in detail and is being used to produce dissimilar aluminum to copper foil single lap joints. A three dimensional finite element model has been developed to study the thermo-mechanical characteristics of the dissimilar Al/Cu single lap joint. The effects of thermal stress and strain have been analyzed by carrying out transient thermal analysis on the heated plates used to join the two 0.1mm thin metal foils. Tensile test has been carried out on the foils before joining and after the single Al/Cu lap joints are made, they are subjected to tensile lap-shear test to analyze the effect of heat on the foils. The analyses are designed to assess the mechanical integrity of the foils after the brazing process and understand whether or not the heat treatment has an effect on the fracture modes of the produced specimens.
Abstract: The study of the aerodynamics related to the
improvement in the acting of airplanes and automobiles with the
objective of being reduced the effect of the attrition of the air on
structures, providing larger speeds and smaller consumption of fuel.
The application of the knowledge of the aerodynamics not more
limits to the aeronautical and automobile industries. Therefore, this
research aims to design and construction of a wind tunnel to perform
aerodynamic analysis in bodies of cars, seeking greater efficiency.
Therefore, this research aims to design and construction of a wind
tunnel to perform aerodynamic analysis in bodies of cars, seeking
greater efficiency. For this, a methodology for wind tunnel type
selection is designed to be built, taking into account the various
existing configurations in which chose to build an open circuit tunnel,
due to the lower complexity of construction and installation;
operational simplicity and low cost. The guidelines for the project
were teaching: the layer that limits study and analyze specimens with
different geometries. For the variation of pressure in the test, section
of a switched gauge used a pitot tube. Thus, it was possible to obtain
quantitative and qualitative results, which proved to be satisfactory.
Abstract: This paper presents the experimental results of 11 kV
and 33 kV silicon composite insulators under artificial salt and urea
polluted conditions. The tests were carried out under different
seasons like summer, winter, and monsoon. The artificial pollution is
prepared by properly dissolving the salt and urea in the water. The
prepared salt and urea pollutions are sprayed on the insulators and
dried up for sufficiently large time. The process is continued until a
uniform layer is formed on the surface of insulator. For each insulator
rating, four samples were tested. The maximum leakage current and
breakdown voltage were measured. From experimental data,
performance of test specimen is evaluated by comparing breakdown
voltage and leakage current during different seasons when exposed to
salt and urea polluted conditions. From these results the performance
of the insulators can be predicted when they are installed in
industrial, agricultural, and coastal areas. The experimental tests were
carried out in the High Voltage laboratory using two stage cascade
transformer having the rating of 1000 kVA, 500 kV.
Abstract: Earth structures constructed of marine clay soils have
tendency to crack. In order to improve the flexural strength and
brittleness, a technique of mixing short fibers is introduced to the soil
lime mixture. Coir fiber was used in this study as reinforcing
elements. An experimental investigation consisting primarily of
flexural tensile tests was conducted to examine the influence of coir
fibers on the flexural behaviour of the reinforced soils. The test
results that the coir fibers were effective in improving the flexural
strength and Young’s modulus of all soils examined and ductility
after peak strength for reinforced marine clay soil treated by lime. 5%
lime treated soil and 1% coir fiber reinforced soil specimens’
demonstrated good strength and durability when submerged in water
and retained 45% of their air-cured strengths.