Abstract: A new reverse phase-high performance liquid chromatography (RP-HPLC) method with fluorescent detector (FLD) was developed and optimized for Norfloxacin determination in human plasma. Mobile phase specifications, extraction method and excitation and emission wavelengths were varied for optimization. HPLC system contained a reverse phase C18 (5 μm, 4.6 mm×150 mm) column with FLD operated at excitation 330 nm and emission 440 nm. The optimized mobile phase consisted of 14% acetonitrile in buffer solution. The aqueous phase was prepared by mixing 2g of citric acid, 2g sodium acetate and 1 ml of triethylamine in 1 L of Milli-Q water was run at a flow rate of 1.2 mL/min. The standard curve was linear for the range tested (0.156–20 μg/mL) and the coefficient of determination was 0.9978. Aceclofenac sodium was used as internal standard. A detection limit of 0.078 μg/mL was achieved. Run time was set at 10 minutes because retention time of norfloxacin was 0.99 min. which shows the rapidness of this method of analysis. The present assay showed good accuracy, precision and sensitivity for Norfloxacin determination in human plasma with a new internal standard and can be applied pharmacokinetic evaluation of Norfloxacin tablets after oral administration in human.
Abstract: The image segmentation method described in this
paper has been developed as a pre-processing stage to be used in
methodologies and tools for video/image indexing and retrieval by
content. This method solves the problem of whole objects extraction
from background and it produces images of single complete objects
from videos or photos. The extracted images are used for calculating
the object visual features necessary for both indexing and retrieval
processes.
The segmentation algorithm is based on the cooperation among an
optical flow evaluation method, edge detection and region growing
procedures. The optical flow estimator belongs to the class of
differential methods. It permits to detect motions ranging from a
fraction of a pixel to a few pixels per frame, achieving good results in
presence of noise without the need of a filtering pre-processing stage
and includes a specialised model for moving object detection.
The first task of the presented method exploits the cues from
motion analysis for moving areas detection. Objects and background
are then refined using respectively edge detection and seeded region
growing procedures. All the tasks are iteratively performed until
objects and background are completely resolved.
The method has been applied to a variety of indoor and outdoor
scenes where objects of different type and shape are represented on
variously textured background.
Abstract: Structured catalysts formed from the growth of
zeolites on substrates is an area of increasing interest due to the
increased efficiency of the catalytic process, and the ability to
provide superior heat transfer and thermal conductivity for both
exothermic and endothermic processes.
However, the generation of structured catalysts represents a
significant challenge when balancing the relationship variables
between materials properties and catalytic performance, with the
Na2O, H2O and Al2O3 gel composition paying a significant role in
this dynamic, thereby affecting the both the type and range of
application.
The structured catalyst films generated as part of this
investigation have been characterised using a range of techniques,
including X-ray diffraction (XRD), Electron microscopy (SEM),
Energy Dispersive X-ray analysis (EDX) and Thermogravimetric
Analysis (TGA), with the transition from oxide-on-alloy wires to
hydrothermally synthesised uniformly zeolite coated surfaces being
demonstrated using both SEM and XRD. The robustness of the
coatings has been ascertained by subjecting these to thermal cycling
(ambient to 550oC), with the results indicating that the synthesis time
and gel compositions have a crucial effect on the quality of zeolite
growth on the FeCrAlloy wires.
Finally, the activity of the structured catalyst was verified by a
series of comparison experiments with standard zeolite Y catalysts in
powdered pelleted forms.
Abstract: In this work we present a solution for DAGC (Digital
Automatic Gain Control) in WLAN receivers compatible to IEEE 802.11a/g standard. Those standards define communication in 5/2.4
GHz band using Orthogonal Frequency Division Multiplexing OFDM modulation scheme. WLAN Transceiver that we have used
enables gain control over Low Noise Amplifier (LNA) and a
Variable Gain Amplifier (VGA). The control over those signals is
performed in our digital baseband processor using dedicated hardware block DAGC. DAGC in this process is used to automatically control the VGA and LNA in order to achieve better
signal-to-noise ratio, decrease FER (Frame Error Rate) and hold the
average power of the baseband signal close to the desired set point.
DAGC function in baseband processor is done in few steps: measuring power levels of baseband samples of an RF signal,accumulating the differences between the measured power level and
actual gain setting, adjusting a gain factor of the accumulation, and
applying the adjusted gain factor the baseband values. Based on the measurement results of RSSI signal dependence to input power we have concluded that this digital AGC can be implemented applying
the simple linearization of the RSSI. This solution is very simple but also effective and reduces complexity and power consumption of the
DAGC. This DAGC is implemented and tested both in FPGA and in ASIC as a part of our WLAN baseband processor. Finally, we have integrated this circuit in a compact WLAN PCMCIA board based on MAC and baseband ASIC chips designed from us.
Abstract: In today scenario, to meet enhanced demand imposed
by domestic, commercial and industrial consumers, various
operational & control activities of Radial Distribution Network
(RDN) requires a focused attention. Irrespective of sub-domains
research aspects of RDN like network reconfiguration, reactive
power compensation and economic load scheduling etc, network
performance parameters are usually estimated by an iterative process
and is commonly known as load (power) flow algorithm. In this
paper, a simple mechanism is presented to implement the load flow
analysis (LFA) algorithm. The reported algorithm utilizes graph
theory principles and is tested on a 69- bus RDN.
Abstract: This paper presents the novel Rao-Blackwellised
particle filter (RBPF) for mobile robot simultaneous localization and
mapping (SLAM) using monocular vision. The particle filter is
combined with unscented Kalman filter (UKF) to extending the path
posterior by sampling new poses that integrate the current observation
which drastically reduces the uncertainty about the robot pose. The
landmark position estimation and update is also implemented through
UKF. Furthermore, the number of resampling steps is determined
adaptively, which seriously reduces the particle depletion problem,
and introducing the evolution strategies (ES) for avoiding particle
impoverishment. The 3D natural point landmarks are structured with
matching Scale Invariant Feature Transform (SIFT) feature pairs. The
matching for multi-dimension SIFT features is implemented with a
KD-Tree in the time cost of O(log2
N). Experiment results on real robot
in our indoor environment show the advantages of our methods over
previous approaches.
Abstract: Depression is a serious mental health problem that
affects people of all ages, including children and adolescents. Studies
showed that female gender is one of the risk factors may influence
the development of depression in adolescents. However, some of the
studies from Turkey suggested that gender does not lead to any
significant difference in the youth depression level. Therefore, the
presented study investigated whether girls differ from boys in respect
of depression. The association between genders and test scores for
the adolescents in a population of primary and secondary school
students was also evaluated. The study was consisting of 254
adolescents (122 boys and 132 girls) with a mean age of 13.86±1.43
(Mean±SD) ranging from 12-16 years. Psychological assessment was
performed using Children-s Depression Inventory (CDI). Chi-square
and Student-s t-test statistics were employed to analyze the data. The
mean of the CDI scores of the girls were higher than boys- CDI
scores (t = -4.580, p = 0.001). Higher ratio appeared for the girls
when they compared with boy group-s depression levels using a CDI
cut-off point of 19 (p = 0.001, Odds Ratio = 2,603). The findings of
the present study suggested that adolescent girls have high level of
depression than adolescent boys aged between 12-16 years in
Turkey. Although some studies reported that there is no any
differences depression level between adolescent boys and girls in
Turkey, result of the present study showed that adolescent girls have
high level of depression than adolescent boys in Turkey.
Abstract: An early and accurate detection of Alzheimer's disease (AD) is an important stage in the treatment of individuals suffering from AD. We present an approach based on the use of structural magnetic resonance imaging (sMRI) phase images to distinguish between normal controls (NC), mild cognitive impairment (MCI) and AD patients with clinical dementia rating (CDR) of 1. Independent component analysis (ICA) technique is used for extracting useful features which form the inputs to the support vector machines (SVM), K nearest neighbour (kNN) and multilayer artificial neural network (ANN) classifiers to discriminate between the three classes. The obtained results are encouraging in terms of classification accuracy and effectively ascertain the usefulness of phase images for the classification of different stages of Alzheimer-s disease.
Abstract: This paper presents a new algorithm which yields a nonlinear state estimator called iterated unscented Kalman filter. This state estimator makes use of both statistical and analytical linearization techniques in different parts of the filtering process. It outperforms the other three nonlinear state estimators: unscented Kalman filter (UKF), extended Kalman filter (EKF) and iterated extended Kalman filter (IEKF) when there is severe nonlinearity in system equation and less nonlinearity in measurement equation. The algorithm performance has been verified by illustrating some simulation results.
Abstract: This paper presents the 20-GHz fractional PLL (Phase
Locked Loop) circuit for the next generation Wi-Fi by using 90 nm
TSMC process. The newly suggested millimeter wave 16/17
pre-scalar is designed and verified by measurement to make the
fractional PLL having a low quantization noise. The operational
bandwidth of the 60 GHz system is 15 % of the carrier frequency
which requires large value of Kv (VCO control gain) resulting in
degradation of phase noise. To solve this problem, this paper adopts
AFC (Automatic Frequency Controller) controlled 4-bit millimeter
wave VCO with small value of Kv. Also constant Kv is implemented
using 4-bit varactor bank. The measured operational bandwidth is 18.2
~ 23.2 GHz which is 25 % of the carrier frequency. The phase noise of
-58 and -96.2 dBc/Hz at 100 KHz and 1 MHz offset is measured
respectively. The total power consumption of the PLL is only 30 mW.
Abstract: Patients with diabetes are susceptible to chronic foot
wounds which may be difficult to manage and slow to heal.
Diagnosis and treatment currently rely on the subjective judgement of
experienced professionals. An objective method of tissue assessment
is required. In this paper, a data fusion approach was taken to wound
tissue classification. The supervised Maximum Likelihood and
unsupervised Multi-Modal Expectation Maximisation algorithms
were used to classify tissues within simulated wound models by
weighting the contributions of both colour and 3D depth information.
It was found that, at low weightings, depth information could show
significant improvements in classification accuracy when compared
to classification by colour alone, particularly when using the
maximum likelihood method. However, larger weightings were
found to have an entirely negative effect on accuracy.
Abstract: In this paper, we present a cost-effective wireless
distributed load shedding system for non-emergency scenarios. In
power transformer locations where SCADA system cannot be used,
the proposed solution provides a reasonable alternative that combines
the use of microcontrollers and existing GSM infrastructure to send
early warning SMS messages to users advising them to proactively
reduce their power consumption before system capacity is reached
and systematic power shutdown takes place.
A novel communication protocol and message set have been
devised to handle the messaging between the transformer sites, where
the microcontrollers are located and where the measurements take
place, and the central processing site where the database server is
hosted. Moreover, the system sends warning messages to the endusers
mobile devices that are used as communication terminals. The
system has been implemented and tested via different experimental
results.
Abstract: This essay presents applicative methods to reduce human exposure levels in the area around base transceiver stations in a environment with multiple sources based on ITU-T recommendation K.70. An example is presented to understand the mitigation techniques and their results and also to learn how they can be applied, especially in developing countries where there is not much research on non-ionizing radiations.
Abstract: A novel idea presented in this paper is to combine
multihop routing with single-frequency networks (SFNs) for a
broadcasting scenario. An SFN is a set of multiple nodes that transmit
the same data simultaneously, resulting in transmitter macrodiversity.
Two of the most important performance factors of multihop
networks, node reachability and routing robustness, are analyzed.
Simulation results show that our proposed SFN-D routing algorithm
improves the node reachability by 37 percentage points as compared
to non-SFN multihop routing. It shows a diversity gain of 3.7 dB,
meaning that 3.7 dB lower transmission powers are required for the
same reachability. Even better results are possible for larger
networks. If an important node becomes inactive, this algorithm can
find new routes that a non-SFN scheme would not be able to find.
Thus, two of the major problems in multihopping are addressed;
achieving robust routing as well as improving node reachability or
reducing transmission power.
Abstract: It has been defined that the “network is the system".
This implies providing levels of service, reliability, predictability and
availability that are commensurate with or better than those that
individual computers provide today. To provide this requires
integrated network management for interconnected networks of
heterogeneous devices covering both the local campus. In this paper
we are addressing a framework to effectively deal with this issue. It
consists of components and interactions between them which are
required to perform the service fault management. A real-world
scenario is used to derive the requirements which have been applied
to the component identification. An analysis of existing frameworks
and approaches with respect to their applicability to the framework is
also carried out.
Abstract: In IETF RFC 2002, Mobile-IP was developed to
enable Laptobs to maintain Internet connectivity while moving
between subnets. However, the packet loss that comes from
switching subnets arises because network connectivity is lost while
the mobile host registers with the foreign agent and this encounters
large end-to-end packet delays. The criterion to initiate a simple and
fast full-duplex connection between the home agent and foreign
agent, to reduce the roaming duration, is a very important issue to be
considered by a work in this paper. State-transition Petri-Nets of the
modeling scenario-based CIA: communication inter-agents procedure
as an extension to the basic Mobile-IP registration process was
designed and manipulated to describe the system in discrete events.
The heuristic of configuration file during practical Setup session for
registration parameters, on Cisco platform Router-1760 using IOS
12.3 (15)T and TFTP server S/W is created. Finally, stand-alone
performance simulations from Simulink Matlab, within each subnet
and also between subnets, are illustrated for reporting better end-toend
packet delays. Results verified the effectiveness of our Mathcad
analytical manipulation and experimental implementation. It showed
lower values of end-to-end packet delay for Mobile-IP using CIA
procedure-based early registration. Furthermore, it reported packets
flow between subnets to improve losses between subnets.
Abstract: Artificial Intelligence based gaming is an interesting topic in the state-of-art technology. This paper presents an automation of a tradition Omani game, called Al-Hawalees. Its related issues are resolved and implemented using artificial intelligence approach. An AI approach called mini-max procedure is incorporated to make a diverse budges of the on-line gaming. If number of moves increase, time complexity will be increased in terms of propositionally. In order to tackle the time and space complexities, we have employed a back propagation neural network (BPNN) to train in off-line to make a decision for resources required to fulfill the automation of the game. We have utilized Leverberg- Marquardt training in order to get the rapid response during the gaming. A set of optimal moves is determined by the on-line back propagation training fashioned with alpha-beta pruning. The results and analyses reveal that the proposed scheme will be easily incorporated in the on-line scenario with one player against the system.
Abstract: The presented work is motivated by a French law
regarding nuclear waste management. A new conceptual Accelerator
Driven System (ADS) designed for the Minor Actinides (MA)
transmutation has been assessed by numerical simulation. The
MUltiple Spallation Target (MUST) ADS combines high thermal power (up to 1.4 GWth) and high specific power. A 30 mA and 1
GeV proton beam is divided into three secondary beams transmitted on three liquid lead-bismuth spallation targets. Neutron and thermalhydraulic
simulations have been performed with the code MURE, based on the Monte-Carlo transport code MCNPX. A methodology has been developed to define characteristic of the MUST ADS concept according to a specific transmutation scenario. The reference
scenario is based on a MA flux (neptunium, americium and curium)
providing from European Fast Reactor (EPR) and a plutonium multireprocessing
strategy is accounted for. The MUST ADS reference
concept is a sodium cooled fast reactor. The MA fuel at equilibrium is mixed with MgO inert matrix to limit the core reactivity and
improve the fuel thermal conductivity. The fuel is irradiated over five
years. Five years of cooling and two years for the fuel fabrication are
taken into account. The MUST ADS reference concept burns about 50% of the initial MA inventory during a complete cycle. In term of
mass, up to 570 kg/year are transmuted in one concept. The methodology to design the MUST ADS and to calculate fuel
composition at equilibrium is precisely described in the paper. A detailed fuel evolution analysis is performed and the reference scenario is compared to a scenario where only americium transmutation is performed.
Abstract: In this paper, SFQ (Start Time Fair Queuing)
algorithm is analyzed when this is applied in computer networks to
know what kind of behavior the traffic in the net has when different
data sources are managed by the scheduler. Using the NS2 software
the computer networks were simulated to be able to get the graphs
showing the performance of the scheduler. Different traffic sources
were introduced in the scripts, trying to establish the real scenario.
Finally the results were that depending on the data source, the traffic
can be affected in different levels, when Constant Bite Rate is
applied, the scheduler ensures a constant level of data sent and
received, but the truth is that in the real life it is impossible to ensure
a level that resists the changes in work load.
Abstract: A mathematical model for the transmission of SARS is developed. In addition to dividing the population into susceptible (high and low risk), exposed, infected, quarantined, diagnosed and recovered classes, we have included a class called untraced. The model simulates the Gompertz curves which are the best representation of the cumulative numbers of probable SARS cases in Hong Kong and Singapore. The values of the parameters in the model which produces the best fit of the observed data for each city are obtained by using a differential evolution algorithm. It is seen that the values for the parameters needed to simulate the observed daily behaviors of the two epidemics are different.