Abstract: In a competitive production environment, critical
decision making are based on data resulted by random sampling of
product units. Efficiency of these decisions depends on data quality
and also their reliability scale. This point leads to the necessity of a
reliable measurement system. Therefore, the conjecture process and
analysing the errors contributes to a measurement system known as
Measurement System Analysis (MSA). The aim of this research is on
determining the necessity and assurance of extensive development in
analysing measurement systems, particularly with the use of
Repeatability and Reproducibility Gages (GR&R) to improve
physical measurements. Nowadays in productive industries,
repeatability and reproducibility gages released so well but they are
not applicable as well as other measurement system analysis
methods. To get familiar with this method and gain a feedback in
improving measurement systems, this survey would be on
“ANOVA" method as the most widespread way of calculating
Repeatability and Reproducibility (R&R).
Abstract: An HPLC-UV analytical method was developed to
determine ethylenediaminetetraacetic acid (EDTA) in dairy
wastewater and surface water. The optimizing separation was achieved
by reversed–phase ion-pair liquid chromatography on a C18 column
using methanol as mobile phase solvent, tetrabutylammonium bromide
as the ion-pair reagent in pH 3.3 formate buffer solution at a flow rate
of 0.9 mL min-1 with a UV detector at 265 nm. No interference of Ca,
Mg or NO3
- was detected. Method performance was evaluated in terms
of linearity, repeatability and reproducibility. The method detection
limit was 5 μg L-1. The contents of EDTA in dairy effluents were 72 ~
261 μg L-1 at a large dairy site. A change of EDTA concentration was
observed downstream of the dairy effluent discharge, but this was well
under the predicted no effect concentration for aquatic ecosystem.