Study on Extraction of Niobium Oxide from Columbite–Tantalite Concentrate
The principal objective of this study is to be able to
extract niobium oxide from columbite-tantalite concentrate of Thayet
Kon Area in Nay Phi Taw. It is recovered from columbite-tantalite
concentrate which contains 19.29 % Nb2O5.The recovery of niobium
oxide from columbite-tantalite concentrate can be divided into three
main sections, namely, digestion of the concentrate, recovery from
the leached solution and precipitation and calcinations. The
concentrate was digested with hydrofluoric acid and sulfuric acid. Of
the various parameters that effect acidity and time were studied. In
the recovery section solvent extraction process using methyl isobutyl
ketone was investigated. Ammonium hydroxide was used as a
precipitating agent and the precipitate was later calcined. The
percentage of niobium oxide is 74%.
[1] Dennis, W.H. 1961. Metallurgy of the Non-Ferrous Metals. London,
U.K: Sir
[2] Miller, G.L. 1957. Metallurgy of the Rarer Metals-6: Tantalum and
Niobium. Isaac Pitman & Sons LTD
[3] May, S.L, Tews, J.L, and Goff, T.N. Separation of Tantalum from
Columbium by the Hydrofluoric Acid-Sulphuric Acid - Methyl Isobutyl
Ketone System. U.S: Bureau of Mines.
[4] B.W. and E.M .Sherwood.1958. Technology of Columbium (Niobium)
[5] Barton, R. William. Columbium and Tantalum: A Material Survey.
Information Circular 8120.U.S: Bureau of Mine
[6] John Wiley & Sons, INC. 1957. Solvent Extraction in Analytical
Chemistry
[7] Takizawa. 1984. Tantalum and Niobium. Japan: JI CA
[1] Dennis, W.H. 1961. Metallurgy of the Non-Ferrous Metals. London,
U.K: Sir
[2] Miller, G.L. 1957. Metallurgy of the Rarer Metals-6: Tantalum and
Niobium. Isaac Pitman & Sons LTD
[3] May, S.L, Tews, J.L, and Goff, T.N. Separation of Tantalum from
Columbium by the Hydrofluoric Acid-Sulphuric Acid - Methyl Isobutyl
Ketone System. U.S: Bureau of Mines.
[4] B.W. and E.M .Sherwood.1958. Technology of Columbium (Niobium)
[5] Barton, R. William. Columbium and Tantalum: A Material Survey.
Information Circular 8120.U.S: Bureau of Mine
[6] John Wiley & Sons, INC. 1957. Solvent Extraction in Analytical
Chemistry
[7] Takizawa. 1984. Tantalum and Niobium. Japan: JI CA
@article{"International Journal of Chemical, Materials and Biomolecular Sciences:60702", author = "Htet Htike Htwe and Kay Thi Lwin", title = "Study on Extraction of Niobium Oxide from Columbite–Tantalite Concentrate", abstract = "The principal objective of this study is to be able to
extract niobium oxide from columbite-tantalite concentrate of Thayet
Kon Area in Nay Phi Taw. It is recovered from columbite-tantalite
concentrate which contains 19.29 % Nb2O5.The recovery of niobium
oxide from columbite-tantalite concentrate can be divided into three
main sections, namely, digestion of the concentrate, recovery from
the leached solution and precipitation and calcinations. The
concentrate was digested with hydrofluoric acid and sulfuric acid. Of
the various parameters that effect acidity and time were studied. In
the recovery section solvent extraction process using methyl isobutyl
ketone was investigated. Ammonium hydroxide was used as a
precipitating agent and the precipitate was later calcined. The
percentage of niobium oxide is 74%.", keywords = "Calcination, Digestion, Precipitation, SolventExtraction.", volume = "2", number = "10", pages = "238-3", }