Using the Transient Plane Source Method for Measuring Thermal Parameters of Electroceramics
Transient plane source method has been used to
measure the thermal diffusivity and thermal conductivity of a compact
isostatic electroceramics at room temperature. The samples were fired
at temperatures from 100 up to 1320 degrees Celsius in steps of
50. Bulk density and specific heat capacity were also measured with
their corresponding standard uncertainties. The results were compared
with further thermal analysis (dilatometry and thermogravimetry).
Structural processes during firing were discussed.
[1] C. Y. Chen, G. S. Lan and W. H. Tuan, "Microstructural evolution
of mullite during the sintering of kaolin powder compacts”, Ceramics
International, Elsevier, vol. 26, pp. 715–720, 2000
[2] M. Benea and M. Gorea, "Mineralogy and technological properties of
some kaolin types used in the ceramic industry”, Studia Universitatis
Babes¸-Bolyai, Geologia, vol. XLIX, pp. 33–39, 2004
[3] H. Wang, Ch. Li, Z. Peng and S. Zhang, "Characterization and thermal
behavior of kaolin”, Journal of Thermal Analysis and Calorimetry,
Springer, vol. 105, pp. 157–160, 2011
[4] M. S. Karmous, "Theoretical study of kaolinite structure; energy
minimization and crystal properties”, World Journal of Nano Science
and Engineering, Scientific Research, vol. 1, pp. 62–66, 2011
[5] T. Hu´lan, A. Trnı´k, I. Sˇ tubnˇa and I. Medved’, "Thermal and elastic
properties of kaolin Sedlec”, Thermophysics 2013, 18th International
Meeting of Thermophysical Society – Conference Proceedings, Brno
University of Technology, pp. 40–46, 2013
[6] S. E. Gustaffson, "Transient plane source techniques for thermal
conductivity and thermal diffusivity measurements of solid materials”,
Review of Scientific Instruments, vol. 62, pp. 797–804, 1991.
[7] M. K. Gustavsson, E. Karawacki and S. E. Gustafsson, "Thermal
conductivity, thermal diffusivity and specific heat of thin samples from
transient measurements with hot-disk sensors”, Review of Scientific
Instruments, vol. 65, pp. 3856–3859, 1994.
[8] M. M. Suleiman, S. E. Gustafsson and L. Bo¨rjesson, "A practical
cryogenic resistive sensor for thermal conductivity measurements”,
Sensors and Actuactors, vol. 57, 1996
[9] V. Boha´cˇ, M. K. Gustavsson, L’. Kubicˇa´r, S. E. Gustafsson, "Parameter
estimations for measurements of thermal transport properties with the
hot disk thermal constants analyzer”, Review of Scientific Instruments,
Elsevier, vol. 71, pp. 15–19, 2000
[10] M. K. Gustavsson, S. E. Gustafsson, "On power variation in self-heated
thermal sensors”, Thermal Conductivity 27, DEStech Publications, Inc.,
vol. 27, pp. 338–346, 2003.
[11] ISO 22007-2, "Plastics — Determination of thermal conductivity and
thermal diffusivty — Transient plane heat source (hot disc) method”,
Geneva, 2008
[12] P. Johansson, B. Adl-Zarrabi, C. Hagentoft, "Usint transient plane source
sensor for determination of thermal properties of vacuum insulation
panels”, Frontiers of Architectural Research, Higher Education Press,
vol. 1, pp. 334–340, 2012.
[13] R. Coquard, E. Coment, G. Flasquin and D. Baillis, "Analysis of
the hot-disk technique applied to low-density insulating materials”,
International Journal of Thermal Sciences, Elsevier, vol. 65, pp.
242–253, 2013.
[14] Y. Li, Ch. Shi, J. Liu, E. Liu, J. Shao, Z. Chen, D. J. Dorantes-Gonzales
and X. Hu, "Improving the accuracy of the transient plane source
method by correcting probe heat capacity and resistance influences”,
Measurement Science and Technology, IOP Publishing Ltd, vol. 25, 2014
[15] S. Malinaricˇ and P. Diesˇka, "Dynamic measurements of the temperature
coefficient of resistance in the transient plane source method”, Int.
Journal of Thermophysics, Springer, vol. 30, pp. 1557–1567, 2009
[16] S. Malinaricˇ, "Contribution to the transient plane source method for
measuring thermophysical properties of solids”, International Journal
of Thermophysics, Springer, vol. 34, pp. 1953–1961, 2013
[17] P. Pytlı´k and R. Sokola´rˇ, Stavebnı´ keramika – technologie, vlastnosti a
vyuzˇitı´, Akademicke´ nakladatelstvı´ CERM, s.r.o., Brno, 2002
[1] C. Y. Chen, G. S. Lan and W. H. Tuan, "Microstructural evolution
of mullite during the sintering of kaolin powder compacts”, Ceramics
International, Elsevier, vol. 26, pp. 715–720, 2000
[2] M. Benea and M. Gorea, "Mineralogy and technological properties of
some kaolin types used in the ceramic industry”, Studia Universitatis
Babes¸-Bolyai, Geologia, vol. XLIX, pp. 33–39, 2004
[3] H. Wang, Ch. Li, Z. Peng and S. Zhang, "Characterization and thermal
behavior of kaolin”, Journal of Thermal Analysis and Calorimetry,
Springer, vol. 105, pp. 157–160, 2011
[4] M. S. Karmous, "Theoretical study of kaolinite structure; energy
minimization and crystal properties”, World Journal of Nano Science
and Engineering, Scientific Research, vol. 1, pp. 62–66, 2011
[5] T. Hu´lan, A. Trnı´k, I. Sˇ tubnˇa and I. Medved’, "Thermal and elastic
properties of kaolin Sedlec”, Thermophysics 2013, 18th International
Meeting of Thermophysical Society – Conference Proceedings, Brno
University of Technology, pp. 40–46, 2013
[6] S. E. Gustaffson, "Transient plane source techniques for thermal
conductivity and thermal diffusivity measurements of solid materials”,
Review of Scientific Instruments, vol. 62, pp. 797–804, 1991.
[7] M. K. Gustavsson, E. Karawacki and S. E. Gustafsson, "Thermal
conductivity, thermal diffusivity and specific heat of thin samples from
transient measurements with hot-disk sensors”, Review of Scientific
Instruments, vol. 65, pp. 3856–3859, 1994.
[8] M. M. Suleiman, S. E. Gustafsson and L. Bo¨rjesson, "A practical
cryogenic resistive sensor for thermal conductivity measurements”,
Sensors and Actuactors, vol. 57, 1996
[9] V. Boha´cˇ, M. K. Gustavsson, L’. Kubicˇa´r, S. E. Gustafsson, "Parameter
estimations for measurements of thermal transport properties with the
hot disk thermal constants analyzer”, Review of Scientific Instruments,
Elsevier, vol. 71, pp. 15–19, 2000
[10] M. K. Gustavsson, S. E. Gustafsson, "On power variation in self-heated
thermal sensors”, Thermal Conductivity 27, DEStech Publications, Inc.,
vol. 27, pp. 338–346, 2003.
[11] ISO 22007-2, "Plastics — Determination of thermal conductivity and
thermal diffusivty — Transient plane heat source (hot disc) method”,
Geneva, 2008
[12] P. Johansson, B. Adl-Zarrabi, C. Hagentoft, "Usint transient plane source
sensor for determination of thermal properties of vacuum insulation
panels”, Frontiers of Architectural Research, Higher Education Press,
vol. 1, pp. 334–340, 2012.
[13] R. Coquard, E. Coment, G. Flasquin and D. Baillis, "Analysis of
the hot-disk technique applied to low-density insulating materials”,
International Journal of Thermal Sciences, Elsevier, vol. 65, pp.
242–253, 2013.
[14] Y. Li, Ch. Shi, J. Liu, E. Liu, J. Shao, Z. Chen, D. J. Dorantes-Gonzales
and X. Hu, "Improving the accuracy of the transient plane source
method by correcting probe heat capacity and resistance influences”,
Measurement Science and Technology, IOP Publishing Ltd, vol. 25, 2014
[15] S. Malinaricˇ and P. Diesˇka, "Dynamic measurements of the temperature
coefficient of resistance in the transient plane source method”, Int.
Journal of Thermophysics, Springer, vol. 30, pp. 1557–1567, 2009
[16] S. Malinaricˇ, "Contribution to the transient plane source method for
measuring thermophysical properties of solids”, International Journal
of Thermophysics, Springer, vol. 34, pp. 1953–1961, 2013
[17] P. Pytlı´k and R. Sokola´rˇ, Stavebnı´ keramika – technologie, vlastnosti a
vyuzˇitı´, Akademicke´ nakladatelstvı´ CERM, s.r.o., Brno, 2002
@article{"International Journal of Engineering, Mathematical and Physical Sciences:67088", author = "Peter Krupa and Svetozár Malinarič", title = "Using the Transient Plane Source Method for Measuring Thermal Parameters of Electroceramics", abstract = "Transient plane source method has been used to
measure the thermal diffusivity and thermal conductivity of a compact
isostatic electroceramics at room temperature. The samples were fired
at temperatures from 100 up to 1320 degrees Celsius in steps of
50. Bulk density and specific heat capacity were also measured with
their corresponding standard uncertainties. The results were compared
with further thermal analysis (dilatometry and thermogravimetry).
Structural processes during firing were discussed.
", keywords = "TPS method, thermal conductivity, thermal diffusivity, thermal analysis, electroceramics, firing.", volume = "8", number = "5", pages = "739-6", }
