Abstract: Syringe pumps are commonly used for drug delivery in hospitals and clinical environments. These instruments are critical in neonatology and oncology, where any variation in the flow rate and drug dosing quantity can lead to severe incidents and even death of the patient. Therefore it is very important to determine the accuracy and precision of these devices using the suitable calibration methods. The Volume Laboratory of the Portuguese Institute for Quality (LVC/IPQ) uses two different methods to calibrate syringe pumps from 16 nL/min up to 20 mL/min. The Interferometric method uses an interferometer to monitor the distance travelled by a pusher block of the syringe pump in order to determine the flow rate. Therefore, knowing the internal diameter of the syringe with very high precision, the travelled distance, and the time needed for that travelled distance, it was possible to calculate the flow rate of the fluid inside the syringe and its uncertainty. As an alternative to the gravimetric and the interferometric method, a methodology based on the application of optical technology was also developed to measure flow rates. Mainly this method relies on measuring the increase of volume of a drop over time. The objective of this work is to compare the results of the calibration of two syringe pumps using the different methodologies described above. The obtained results were consistent for the three methods used. The uncertainties values were very similar for all the three methods, being higher for the optical drop method due to setup limitations.
Abstract: The tribological tests were performed on a new
tribometer, in order to measure the coefficient of friction of a gland
seal packing material on stainless steel shafts in presence of Cellulose
Nanocrystal (CNC) suspension as a sustainable, environmentally
friendly, water-based lubricant. To simulate the real situation from the
slurry pumps, silica sands were used as slurry particles. The surface
profiles after tests were measured by interferometer microscope to
characterize the surface wear. Moreover, the coefficient of friction
and surface wear were measured between stainless steel shaft and
chrome steel ball to investigate the tribological effects of CNC in
boundary lubrication region. Alignment of nanoparticles in the CNC suspensions are the
main reason for friction and wear reduction. The homogeneous
concentrated suspensions showed fingerprint patterns of a chiral
nematic liquid crystal. These properties made CNC a very good
lubricant additive in water.
Abstract: To provide the conditions for nuclear fusion by high energy and powerful laser beams, it is required to have a high degree of symmetry and surface uniformity of the spherical capsules to reduce the Rayleigh-Taylor hydrodynamic instabilities. In this paper, we have used the digital microscopic holography based on Mach-Zehnder interferometer to study the quality of targets for inertial fusion. The interferometric pattern of the target has been registered by a CCD camera and analyzed by Holovision software. The uniformity of the surface and shell thickness are investigated and measured in reconstructed image. We measured shell thickness in different zone where obtained non uniformity 22.82 percent.
Abstract: The purpose of this project is to propose a quick and
environmentally friendly alternative to measure the quality of oils
used in food industry. There is evidence that repeated and
indiscriminate use of oils in food processing cause physicochemical
changes with formation of potentially toxic compounds that can
affect the health of consumers and cause organoleptic changes. In
order to assess the quality of oils, non-destructive optical techniques
such as Interferometry offer a rapid alternative to the use of reagents,
using only the interaction of light on the oil. Through this project, we
used interferograms of samples of oil placed under different heating
conditions to establish the changes in their quality. These
interferograms were obtained by means of a Mach-Zehnder
Interferometer using a beam of light from a HeNe laser of 10mW at
632.8nm. Each interferogram was captured, analyzed and measured
full width at half-maximum (FWHM) using the software from
Amcap and ImageJ. The total of FWHMs was organized in three
groups. It was observed that the average obtained from each of the
FWHMs of group A shows a behavior that is almost linear, therefore
it is probable that the exposure time is not relevant when the oil is
kept under constant temperature. Group B exhibits a slight
exponential model when temperature raises between 373 K and 393
K. Results of the t-Student show a probability of 95% (0.05) of the
existence of variation in the molecular composition of both samples.
Furthermore, we found a correlation between the Iodine Indexes
(Physicochemical Analysis) and the Interferograms (Optical
Analysis) of group C. Based on these results, this project highlights
the importance of the quality of the oils used in food industry and
shows how Interferometry can be a useful tool for this purpose.
Abstract: Laser interferometric methods have been utilized for the measurement of natural convection heat transfer from a heated vertical flat plate, in the investigation presented here. The study mainly aims at comparing two different fringe orientations in the wedge fringe setting of Mach-Zehnder interferometer (MZI), used for the measurements. The interference fringes are set in horizontal and vertical orientations with respect to the heated surface, and two different fringe analysis methods, namely the stepping method and the method proposed by Naylor and Duarte, are used to obtain the heat transfer coefficients. The experimental system is benchmarked with theoretical results, thus validating its reliability in heat transfer measurements. The interference fringe patterns are analyzed digitally using MATLAB 7 and MOTIC Plus softwares, which ensure improved efficiency in fringe analysis, hence reducing the errors associated with conventional fringe tracing. The work also discuss the relative merits and limitations of the two methods used.
Abstract: Hair is a non homogenous complex material which
can be associated with a polymer. It is made up 95% of Keratin.
Hair has a great social significance for human beings. In the High
Middle Ages, for example, long hairs have been reserved for kings
and nobles.
Most common interest in hair is focused on hair growth, hair types
and hair care, but hair is also an important biomaterial which can
vary depending on ethnic origin or on age, hair colour for example
can be a sign of ethnic ancestry or age (dark hair for Asiatic, blond
hair for Caucasian and white hair for old people in general).
In this context, different approaches have been conducted to
determine the differences in mechanical properties and characterize
the fracture topography at the surface of hair depending on its type
and its age.
A tensile testing machine was especially designed to achieve
tensile tests on hair. This device is composed of a microdisplacement
system and a force sensor whose peak load is limited to
3N. The curves and the values extracted from each experiment, allow
us to compare the evolution of the mechanical properties from one
hair to another.
Observations with a Scanning Electron Microscope (SEM) and
with an interferometer were made on different hairs. Thus, it is
possible to access the cuticle state and the fracture topography for
each category.
Abstract: We investigated statistical performance of Bayesian inference using maximum entropy and MAP estimation for several models which approximated wave-fronts in remote sensing using SAR interferometry. Using Monte Carlo simulation for a set of wave-fronts generated by assumed true prior, we found that the method of maximum entropy realized the optimal performance around the Bayes-optimal conditions by using model of the true prior and the likelihood representing optical measurement due to the interferometer. Also, we found that the MAP estimation regarded as a deterministic limit of maximum entropy almost achieved the same performance as the Bayes-optimal solution for the set of wave-fronts. Then, we clarified that the MAP estimation perfectly carried out phase unwrapping without using prior information, and also that the MAP estimation realized accurate phase unwrapping using conjugate gradient (CG) method, if we assumed the model of the true prior appropriately.
Abstract: In this paper, a fiber based Fabry-Perot interferometer
is proposed and demonstrated for a non-contact displacement
measurement. A piece of micro-prism which attached to the
mechanical vibrator is served as the target reflector. Interference
signal is generated from the superposition between the sensing beam
and the reference beam within the sensing arm of the fiber sensor.
This signal is then converted to the displacement value by using a
developed program written in visual Cµ programming with a
resolution of λ/8. A classical function generator is operated for
controlling the vibrator. By fixing an excitation frequency of 100 Hz
and varying the excitation amplitude range of 0.1 – 3 Volts, the
output displacements measured by the fiber sensor are obtained from
1.55 μm to 30.225 μm. A reference displacement sensor with a
sensitivity of ~0.4 μm is also employed for comparing the
displacement errors between both sensors. We found that over the
entire displacement range, a maximum and average measurement
error are obtained of 0.977% and 0.44% respectively.
Abstract: This paper describes a method to measure and
compensate a 4 axes ultra-precision machine tool that generates micro
patterns on the large surfaces. The grooving machine is usually used
for making a micro mold for many electrical parts such as a light guide
plate for LCD and fuel cells. The ultra precision machine tool has three
linear axes and one rotational table. Shaping is usually used to
generate micro patterns. In the case of 50 μm pitch and 25 μm height
pyramid pattern machining with a 90° wedge angle bite, one of linear
axis is used for long stroke motion for high cutting speed and other
linear axis are used for feeding. The triangular patterns can be
generated with many times of long stroke of one axis. Then 90°
rotation of work piece is needed to make pyramid patterns with
superposition of machined two triangular patterns.
To make a two dimensional positioning error, straightness of two
axes in out of plane, squareness between the each axis are important.
Positioning errors, straightness and squarness were measured by laser
interferometer system. Those were compensated and confirmed by
ISO230-6. One of difficult problem to measure the error motions is
squareness or parallelism of axis between the rotational table and
linear axis. It was investigated by simultaneous moving of rotary table
and XY axes. This compensation method is introduced in this paper.
Abstract: The presented paper shows the possibility of using
holographic interferometry for measurement of temperature field in
moving fluids. There are a few methods for identification of velocity
fields in fluids, such us LDA, PIV, hot wire anemometry. It is very
difficult to measure the temperature field in moving fluids. One of the
often used methods is Constant Current Anemometry (CCA), which
is a point temperature measurement method. Data are possibly
acquired at frequencies up to 1000Hz. This frequency should be
limiting factor for using of CCA in fluid when fast change of
temperature occurs. This shortcoming of CCA measurements should
be overcome by using of optical methods such as holographic
interferometry. It is necessary to employ a special holographic setup
with double sensitivity instead of the commonly used Mach-Zehnder
type of holographic interferometer in order to attain the parameters
sufficient for the studied case. This setup is not light efficient like the
Mach-Zehnder type but has double sensitivity. The special technique
of acquiring and phase averaging of results from holographic
interferometry is also presented. The results from the holographic
interferometry experiments will be compared with the temperature
field achieved by methods CCA method.
Abstract: An optical fiber Fabry-Perot interferometer (FFPI) is
proposed and demonstrated for dynamic measurements in a
mechanical vibrating target. A polishing metal with a low reflectance
value adhered to a mechanical vibrator was excited via a function
generator at various excitation frequencies. Output interference
fringes were generated by modulating the reference and sensing
signal at the output arm. A fringe-counting technique was used for
interpreting the displacement information on the dedicated computer.
The fiber interferometer has been found the capability of the
displacement measurements of 1.28 μm – 96.01 μm. A commercial
displacement sensor was employed as a reference sensor for
investigating the measurement errors from the fiber sensor. A
maximum percentage measurement error of approximately 1.59 %
was obtained.
Abstract: In this paper, by exploiting a single semiconductor
optical amplifier-Mach Zehnder Interferometer (SOA-MZI), an
integratable all-optical flip-flop (AOFF) is proposed. It is composed
of a SOA-MZI with a bidirectional coupler at the output. Output
signals of both bar and crossbar of the SOA-MZI is fed back to SOAs
located in the arms of the Mach-Zehnder Interferometer (MZI). The
injected photon-rates to the SOAs are modulated by feedback signals
in order to form optical flip-flop. According to numerical analysis,
Gaussian optical pulses with the energy of 15.2 fJ and 20 ps duration
with the full width at half-maximum criterion, can switch the states of
the SR-AOFF. Also simulation results show that the SR-AOFF has
the contrast ratio of 8.5 dB between two states with the transition
time of nearly 20 ps.
Abstract: We demonstrate single-photon interference over 10 km using a plug and play system for quantum key distribution. The quality of the interferometer is measured by using the interferometer
visibility. The coding of the signal is based on the phase coding and the value of visibility is based on the interference effect, which result a number of count. The setup gives full control of polarization inside
the interferometer. The quality measurement of the interferometer is based on number of count per second and the system produces 94 % visibility in one of the detectors.